G‐SERF Editing in Two‐Dimensional Pure‐Shift Total Correlation Spectroscopy: Scalar Coupling Measurements for a Group of Spins in Organic Molecules          href='#cphc201900174-note-1001'/>

Rao?Kakita Veera Mohana; Joshi Mamata V; Hosur Ramakrishna V

摘要

Abstract >A novel G‐SERF‐PSYCHE‐TOCSY (gradient encoded selective refocusing in pure shift yielded by chirp excitation version of total correlation spectroscopy) NMR pulse scheme has been proposed, which produces TOCSY chemical shift correlations, on one hand, and scalar coupling values for the spins scalarly coupled to irradiated resonances, by showing them as doublets along the indirect dimension, on the other. Therefore, recording such an experiment, for a group of spins with overlapping chemical shifts, in organic molecules can adequately provide scalar coupling information in a G‐SERF manner along the indirect dimensions, and they can be assigned to particular spin pairs. Such COSY chemical shift correlations (which appear as doublets for the scalarly coupled spins) can be readily discriminated from the TOCSY peaks (which do not show such splitting) in the G‐SERF‐PSYCHE‐TOCSY spectrum. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <title类型=“main”>抽象</ title> >一种新颖的g-serf-spey-tocsy（纯粹编码选择性重新聚焦纯换档）已经提出了总相关光谱的Chirp激励版本的总相关光谱分程），通过将旋转耦合到照射的共振的旋转的旋转的标量耦合值来提出了NMR脉冲方案。另一个。因此，在有机分子中记录这种实验，对于具有重叠化学变换的一组旋转，可以在有机分子中充分地以间接尺寸以G-Serf方式提供标量耦合信息，并且它们可以被分配给特定的自旋对。这种舒适的化学移位相关性（显现为标定耦合旋转的双峰）可以容易地区别于G-SERF-PSPYCE-TOCSY频谱中的Tocsy峰（不显示这种分裂）。</ p> </ abstract > </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16300/'>《Chemphyschem: A European journal of chemical physics and physical chemistry》</a> <b style="margin: 0 2px;">|</b><span>2019年第12期</span><b style="margin: 0 2px;">|</b><span>共8页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Rao?Kakita Veera Mohana&option=202" target="_blank" rel="nofollow">Rao?Kakita Veera Mohana;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Joshi Mamata V&option=202" target="_blank" rel="nofollow">Joshi Mamata V;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Hosur Ramakrishna V&option=202" target="_blank" rel="nofollow">Hosur Ramakrishna V;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>UM-DAE-Centre for Excellence in Basic SciencesUniversity of Mumbai Kalina Campus SantacruzMumbai 400 098 India;</p> <p>Department of Chemical SciencesTata Institute of Fundamental Research (TIFR)1-Homi Bhabha Road Colaba Mumbai 400 005 India;</p> <p>UM-DAE-Centre for Excellence in Basic SciencesUniversity of Mumbai Kalina Campus SantacruzMumbai 400 098 India;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=homodecoupling&option=203" rel="nofollow">homodecoupling;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nuclear magnetic resonance&option=203" rel="nofollow">nuclear magnetic resonance;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=organic molecules&option=203" rel="nofollow">organic molecules;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=scalar couplings&option=203" rel="nofollow">scalar couplings;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=total correlation spectroscopy&option=203" rel="nofollow">total correlation spectroscopy;</a> </p> <div class="translation"> 机译：同源耦合;核磁共振;有机分子;标量联轴器;总相关光谱; 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href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=曲景奎&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,曲景奎</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=余志辉&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,余志辉</a> <span> <a href="/journal-cn-10804/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 分析化学 </a> </span> <span> . 2019</span><span>,第003期</span> </span> </div> </li> <li> <div> <b>6. </b><a class="enjiyixqcontent" href="/academic-conference-cn_meeting-7975_thesis/020222035449.html">氢化物发生-电感耦合等离子体原子发射光谱法测定高纯锡中痕量砷</a> <b>[C]</b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=戴凤英&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 戴凤英</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=刘天平&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,刘天平</a> <span> <a href="/conference-cn-7975/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 全国有色金属理化检验学术报告会 </a> <span> <span> . 2012</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/020314372161.html">运用二维相关荧光光谱法分析混合体系中微量物质的研究</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=倪磊&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 倪磊</a> <span> . 2019</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/06120103947019.html">采用微波消解辅助电感耦合等离子体发射光谱法测定纺织品中总锌含量的方法</a> <b>[P]</b> . <span> 中国专利： CN111307788A </span> <span> . 2020-06-19</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120105191533.html">借助测量光谱与参照光谱的互相关来测定均匀分布在介质中的化学物质的存在的方法</a> <b>[P]</b> . <span> 中国专利： CN1989408A </span> <span> . 2007-06-27</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130450068464.html">Application of two-dimensional heteronuclear correlation spectroscopy to investigate solid samples containing hydrogen and carbon nuclei, with chemical shift correlation by scalar coupling</a> <b>[P]</b> . <span> 外国专利：  DE19834145C1 </span> <span> . 2000-03-09</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：二维异核相关光谱在研究含氢和碳核的固体样品中的应用，通过标量耦合进行化学位移相关 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130442453990.html">USE OF TWO-DIMENSIONAL 15N/1H NMR CORRELATION SPECTROSCOPY IN A PROCESS FOR DESIGNING HIGH-AFFINITY LIGANDS TO TARGET MOLECULES</a> <b>[P]</b> . <span> 外国专利：  IL123572A </span> <span> . 2004-06-01</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：二维15 N / 1 H NMR关联光谱在设计目标分子的高亲和力过程中的应用 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130442450592.html">USE OF TWO-DIMENSIONAL 15N/1H NMR CORRELATION SPECTROSCOPY IN A PROCESS FOR DESIGNING HIGH-AFFINITY LIGANDS TO TARGET MOLECULES</a> <b>[P]</b> . <span> 外国专利：  IL149512B </span> <span> . 2004-06-01</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：二维15N / 1H NMR关联光谱在设计目标分子的高亲和力过程中的应用 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div 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