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首页> 外文期刊>ChemElectroChem >Synthesis of Off‐Stoichiometric CoS Nanoplates from a Molecular Precursor for Efficient H2/O2 Evolution and Supercapacitance
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Synthesis of Off‐Stoichiometric CoS Nanoplates from a Molecular Precursor for Efficient H2/O2 Evolution and Supercapacitance

机译：从分子前体合成脱离化学计量COS纳米烯，以高效H2 / O2进化和超水分

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Abstract > The development of cost‐effective and easily accessible bifunctional materials, which can be effectively used for energy storage and energy generation, is highly desirable. Herein, a new molecular precursor [ tris (morpholinodithiocarbamato)Co(III)] has been synthesized and the X‐ray crystal structure of the complex determined. The precursor was used to prepare oleylamine (OLA)‐capped cobalt sulfide nanoplatelets, using a facile hot injection method at two different temperatures (200?°C and 260?°C). The characterization of the samples shows that CoS synthesized at 200?°C is slightly sulfur rich, whereas CoS synthesized at 260?°C is slightly cobalt rich. The effect of off‐stoichiometry of CoS nanoplatelets on the energy generation and storage applications was studied. The oxygen evolution reaction catalytic performance of both samples indicate overpotentials of 307 and 276?mV as well as Tafel slopes of 96 and 82?mV/dec, respectively. Similarly, overpotentials of 132 and 153?mV were observed for the hydrogen evolution reaction, with Tafel slopes of 159 and 154?mV/dec, respectively. The capacitive behavior of the samples was also examined, and specific capacitance values of 298 and 440?F/g were obtained with cycling stabilities of 73 and 97?%, after 5000 cycles, respectively. The results indicate that sulfur‐deficient CoS can show superior performance for efficient energy generation and storage devices. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> > 能够有效地用于储能和能量产生的成本效益和易于接近的双功能材料的开发是非常理想的。在此，新的分子前体[ tris </ i> （吗啉代硫代氨基甲酰胺）CO（III）]已被合成，并测定复合物的X射线晶体结构。使用两个不同温度（200℃和260℃）的容易热注射方法，使用前体制备油胺（OLA）硫化物硫化物纳米孔。样品的表征表明，在200℃合成的COS合成浓度富含硫，而在260℃下合成的COS略带富含钴。研究了COS纳米孔的偏离化学计量对能量产生和储存应用的影响。两种样品的氧气逸出反应催化性能分别表示307和276Ωmv以及96和82℃的Tafel斜率的过电。类似地，对于氢进化反应，观察到132和153？MV的过电位，Tafel斜率分别为159和154〜12月。还检查了样品的电容性能，并且在5000次循环后，通过循环稳定性为73和97Ω％的循环稳定性而获得特定电容值。结果表明，硫缺陷COS可以显示出高效的能量产生和存储设备的卓越性能。 </ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" >著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16042/'>《ChemElectroChem》</a> <b style="margin: 0 2px;">|</b><span>2019年第9期</span><b style="margin: 0 2px;">|</b><span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gervas Charles&option=202" target="_blank" rel="nofollow">Gervas Charles;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Khan Malik Dilshad&option=202" target="_blank" rel="nofollow">Khan Malik Dilshad;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mlowe Sixberth&option=202" target="_blank" rel="nofollow">Mlowe Sixberth;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhang Chunyang&option=202" target="_blank" rel="nofollow">Zhang Chunyang;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Zhao Chen&option=202" target="_blank" rel="nofollow">Zhao Chen;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Gupta Ram K.&option=202" target="_blank" rel="nofollow">Gupta Ram K.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Akerman Matthew P.&option=202" target="_blank" rel="nofollow">Akerman Matthew P.;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Mashazi Philani&option=202" target="_blank" rel="nofollow">Mashazi Philani;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Nyokong Tebello&option=202" target="_blank" rel="nofollow">Nyokong Tebello;</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Revaprasadu Neerish&option=202" target="_blank" rel="nofollow">Revaprasadu Neerish;</a> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> <p>Department of ChemistryUniversity of ZululandPrivate bag X1001 Kwa-Dlangezwa 3880 South Africa;</p> <p>Department of ChemistryUniversity of ZululandPrivate bag X1001 Kwa-Dlangezwa 3880 South Africa;</p> <p>Department of ChemistryUniversity of ZululandPrivate bag X1001 Kwa-Dlangezwa 3880 South Africa;</p> <p>Department of ChemistryPittsburg State UniversityPittsburg Kansas USA;</p> <p>Department of ChemistryPittsburg State UniversityPittsburg Kansas USA;</p> <p>Department of ChemistryPittsburg State UniversityPittsburg Kansas USA;</p> <p>School of Chemistry and PhysicsPrivate Bag X01 Scottsville Pietermaritzburg South Africa;</p> <p>Department of ChemistryRhodes UniversityPO Box 94 Grahamstown 6140 South Africa;</p> <p>Department of ChemistryRhodes UniversityPO Box 94 Grahamstown 6140 South Africa;</p> <p>Department of ChemistryUniversity of ZululandPrivate bag X1001 Kwa-Dlangezwa 3880 South Africa;</p> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li > <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span><a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=energy generation&option=203" rel="nofollow">energy generation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=energy storage&option=203" rel="nofollow">energy storage;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=hydrogen evolution&option=203" rel="nofollow">hydrogen evolution;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=oxygen evolution&option=203" rel="nofollow">oxygen evolution;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=supercapacitance&option=203" rel="nofollow">supercapacitance;</a> </p> <div class="translation"> 机译：能量产生;储能;氢气进化;氧气进化;超级电容; </div> </li> </ul> </div> </div> <div class="literature cardcommon"> <div class="similarity "> <h3 class="all_title" id="enpatent66">相似文献</h3> <div class="similaritytab clearfix"> <ul> <li class="active" >外文文献</li> <li >中文文献</li> <li >专利</li> </ul> </div> <div class="similarity_details"> <ul > <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/journal-foreign-detail/0704022061831.html">Synthesis of Off‐Stoichiometric CoS Nanoplates from 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. <span> 外国专利： <!-- 韩国专利： --> KR1015156770000B1 </span> <span> . 2015-05-11</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用高均匀钯纳米粒子由H2和O2直接合成H2O2的方法 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130478900721.html">PROCESS FOR THE PURIFICATION OF A H2S, CO2 AND H2O CONTAINING NATURAL GAS FLOW, BY ADSORPTION TO A ZEOLITIC MOLECULAR SIEVE MATERIAL AND REGENERATION OF THIS SIEVE MATERIAL.</a> <b>[P]</b> . <span> 外国专利： <!-- --> NL160794C </span> <span> . 1979-12-17</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：通过吸附到分子筛材料和再生该筛子的方法纯化含H2S，CO2和H2O的天然气流。 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" 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