Correlative Multiscale 3D Imaging of a Hierarchical Nanoporous Gold Catalyst by Electron, Ion and X‐ray Nanotomography

摘要

Abstract >Tomographic imaging of catalysts allows non‐invasive investigation of structural features and chemical properties by combining large fields of view, high spatial resolution, and the ability to probe multiple length scales. Three complementary nanotomography techniques, (i)?electron tomography, (ii)?focused ion beam—scanning electron microscopy, and (iii)?synchrotron ptychographic X‐ray computed tomography, were applied to render the 3D structure of monolithic nanoporous gold doped with ceria, a catalytically active material with hierarchical porosity on the nm and μm scale. The resulting tomograms were used to directly measure volume fraction, surface area and pore size distribution, together with 3D pore network mapping. Each technique is critically assessed in terms of approximate spatial resolution, field of view, sample preparation and data processing requirements. Ptychographic X‐ray computed tomography produced 3D electron density maps with isotropic spatial resolution of 23?nm, the highest so far demonstrated for a catalyst material, and is highlighted as an emerging method with excellent potential in the field of catalysis. </abstract> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> <div class="translation abstracttxt"> <span class="zhankaihshouqi fivelineshidden" id="abstract"> <span>机译：</span><Abstract Type =“Main”XML：Lang =“en”> <标题类型=“main”>抽象</ title> >催化剂的断层摄影通过组合大型视野，高空间分辨率和探测多个长度尺度的能力来允许非侵入性研究结构特征和化学性质。三种互补纳米分析技术，（i）？电子断层扫描，（ii）α聚焦离子束扫描电子显微镜，（iii）？Synchrotron Ptychographic X射线计算断层扫描，呈现出单片纳米多孔金的3D结构掺杂Ceria，一种催化活性材料，Nm和μm的分层孔隙率。得到的断层图像用于直接测量体积分数，表面积和孔径分布，以及3D孔网络映射。在近似空间分辨率，视野，样品准备和数据处理要求方面，每种技术都受到严格评估。 Ptychographic X射线计算机断层扫描产生3D电子密度图，具有23Ω·Nm的各向同性空间分辨率，最高的是催化剂材料的最高，并且被突出显示为催化方法，在催化领域具有出色的潜力。</ p> </摘要> </span> <span class="z_kbtn z_kbtnclass hoverxs" style="display: none;">展开▼</span> </div> </div> <div class="record"> <h2 class="all_title" id="enpatent33" > 著录项</h2> <ul> <li> <span class="lefttit">来源</span> <div style="width: 86%;vertical-align: text-top;display: inline-block;"> <a href='/journal-foreign-16041/'>《ChemCatChem 》</a> <b style="margin: 0 2px;">|</b><span>2018年第13期</span><b style="margin: 0 2px;">|</b> <span>共10页</span> </div> </li> <li> <div class="author"> <span class="lefttit">作者</span> <p id="fAuthorthree" class="threelineshidden zhankaihshouqi"> </p> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zkzz" style="display: none;">展开▼</span> </div> </li> <li> <div style="display: flex;"> <span class="lefttit">作者单位</span> <div style="position: relative;margin-left: 3px;max-width: 639px;"> <div class="threelineshidden zhankaihshouqi" id="fOrgthree"> </div> <span class="z_kbtnclass z_kbtnclassall hoverxs" id="zhdw" style="display: none;">展开▼</span> </div> </div> </li> <li> <span class="lefttit">收录信息</span> <span style="width: 86%;vertical-align: text-top;display: inline-block;"></span> </li> <li> <span class="lefttit">原文格式</span> <span>PDF</span> </li> <li> <span class="lefttit">正文语种</span> <span>eng</span> </li> <li> <span class="lefttit">中图分类</span> <span> <a href="https://www.zhangqiaokeyan.com/clc/1186.html" title="物理化学（理论化学）、化学物理学">物理化学（理论化学）、化学物理学 ;</a></span> </li> <li class="antistop"> <span class="lefttit">关键词</span> <p style="width: 86%;vertical-align: text-top;"> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=electron microscopy&option=203" rel="nofollow">electron microscopy;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=nanomaterials&option=203" rel="nofollow">nanomaterials;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=ptychography&option=203" rel="nofollow">ptychography;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=synchrotron radiation&option=203" rel="nofollow">synchrotron radiation;</a> <a style="color: #3E7FEB;" href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=tomography&option=203" rel="nofollow">tomography;</a> </p> <div class="translation"> 机译：电子显微镜;纳米材料;ptychography;同步辐射;断层扫描; 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Li Ruizhe</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=李睿哲&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,李睿哲</a> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=Li Liang&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor">,Li Liang</a> <span> <a href="/conference-cn-1411/" target="_blank" rel="nofollow" class="tuijian_authcolor"> . 第十四届中国体视学与图像分析学术会议 </a> <span> <span> . 2015</span> </span> </div> </li> <li> <div> <b>7. </b><a class="enjiyixqcontent" href="/academic-degree-domestic_mphd_thesis/02031635789.html">波带板X射线成像与电子散射用于等离子体高空间分辨诊断的数值模拟</a> <b>[A] </b> <span> <a href="/search.html?doctypes=4_5_6_1-0_4-0_1_2_3_7_9&sertext=陈晓虎&option=202" target="_blank" rel="nofollow" class="tuijian_auth tuijian_authcolor"> . 陈晓虎</a> <span> . 2015</span> </span> </div> </li> </ul> <ul style="display: none;"> <li> <div> <b>1. </b><a class="enjiyixqcontent" href="/patent-detail/061203366894.html">聚焦离子束—氦离子显微镜对页岩纳米孔隙三维成像方法</a> <b>[P]</b> . <span> 中国专利： CN109298005B </span> <span> . 2019.06.28</span> </div> </li> <li> <div> <b>2. </b><a class="enjiyixqcontent" href="/patent-detail/06120100281067.html">聚焦离子束—氦离子显微镜对页岩纳米孔隙三维成像方法</a> <b>[P]</b> . <span> 中国专利： CN109298005A </span> <span> . 2019-02-01</span> </div> </li> <li> <div> <b>3. </b><a class="enjiyixqcontent" href="/patent-detail/06130411540563.html">CORRELATIVE MICROSCOPY OF LIGHT MICROSCOPE AND ELECTRON MICROSCOPE USING A WORK STATION COMPRISING SAMPLE HOLDER FOR CRYOGENIC ELECTRON MICROSCOPY FOR CORRELATIVE IMAGING DETECTION APPARATUS IN COMBINATION OF OPTICAL MICROSCOPY AND ELECTRON MICROSCOPY OR CORRELATIVE IMAGING DETECTION INCLUDING SAID WORK STATION</a> <b>[P]</b> . <span> 外国专利：  KR20160016399A </span> <span> . 2016-02-15</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：光学显微镜和电子显微镜的相关显微技术，包括一个工作台，包括用于低温电子显微镜的样品夹持器，用于光学成像和电子显微镜，光学显微镜，光学显微镜和光学显微镜之间的相关成像检测装置 </span> </p> </li> <li> <div> <b>4. </b><a class="enjiyixqcontent" href="/patent-detail/06130411337053.html">Correlative microscopy of light microscope and electron microscope using a work station comprising sample holder for cryogenic electron microscopy for correlative imaging detection apparatus in combination of optical microscopy and electron microscopy or correlative imaging detection including said work station</a> <b>[P]</b> . <span> 外国专利：  KR101672336B1 </span> <span> . 2016-11-04</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：使用工作站的光学显微镜和电子显微镜的相关显微镜，该工作站包括用于低温电子显微镜的样本保持器，用于与光学显微镜和电子显微镜相结合的相关成像检测设备或包括所述工作站的相关成像检测 </span> </p> </li> <li> <div> <b>5. </b><a class="enjiyixqcontent" href="/patent-detail/06130411763077.html">WORK STATION INCLUDING SAMPLE HOLDER FOR CRYOGENIC ELECTRON MICROSCOPE FOR CORRELATIVE IMAGING DETECTION OF LIGHT MICROSCOPE AND ELECTRON MICROSCOPE, CORRELATIVE IMAGING DETECTION APPARATUS INCLUDING SAME, AND IMAGING DETECTION METHOD AND IMAGING SYSTEM USING SAME</a> <b>[P]</b> . <span> 外国专利：  WO2016021745A1 </span> <span> . 2016-02-11</span> </div> <p class="zwjiyix translation" style="max-width: initial;height: auto;word-break: break-all;white-space: initial;text-overflow: initial;overflow: initial;"> <span>机译：包括低温电子显微镜样品架的工作台，用于光显微镜和电子显微镜的相关成像检测，包括相同的相关成像检测装置，以及使用相同方法的成像检测方法和成像系统 </span> </p> </li> </ul> </div> </div> </div> <div class="theme cardcommon" style="overflow: auto;display:none"> <h3 class="all_title" id="enpatent55">相关主题</h3> <ul id="subject"> </ul> </div> </div> </div> </div> <div class="right rightcon"> <div class="details_img cardcommon clearfix" style="margin-bottom: 10px;display:none;" > </div> </div> </div> <div id="thesis_get_original1" class="downloadBth" style="bottom: 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