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Comparative investigation of microstructure and properties of Ni-coated FeSiAl soft magnetic composite coatings produced by cold spraying and HVOF

机译:冷喷涂和HVOF产生的Ni涂层迷裂软磁复合涂层微观结构和性能的比较研究

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摘要

In this work, the techniques of cold spray (CS) and high velocity oxygen-fuel (HVOF) were employed to fabricate Ni/FeSiAl soft magnetic composite (SMC) coatings by using Ni-coated FeSiAl composite powder. The micro-structural features were characterized in terms of scanning electron microscope (SEM) and X-ray diffraction (XRD) analyses. The tribological and magnetic properties of the Ni/FeSiAl SMC coatings were also comparatively studied. Results showed that the CS coating exhibited higher particle deformation and much higher density, whereas the HVOF coating showed more visible defects and slightly higher oxide content. Both CS coating and HVOF coating resulted some loss of FeSiAl particles during deposition, while a higher content of FeSiAl particles was achieved in the HVOF composite coating, indicated a higher deposition efficiency of FeSiAl particles during HVOF deposition. According to the XRD analysis, both SMC coatings had no obvious oxidation and phase transformation during deposition processes. The EDS analysis proved partially melted particles during HVOF deposition. Tribological tests revealed a better wear performance of the CS coating as a result of the enhanced plastic deformation and microhardness. The HVOF coating showed a better magnetic performance, with a lower coercivity and a higher saturation magnetization compared to those of CS coating. This can be explained by a higher retainability of FeSiAl particles and a smaller strain stress generation during HVOF deposition.
机译:在这项工作中,使用冷喷雾(CS)和高速氧气 - 燃料(HVOF)的技术来制造通过使用Ni涂覆的迷裂复合粉末制备Ni /迷裂的软磁复合物(SMC)涂层。在扫描电子显微镜(SEM)和X射线衍射(XRD)分析方面表征了微结构特征。 Ni /雌性SMC涂层的摩擦学和磁性也比较较手。结果表明,Cs涂层表现出更高的颗粒变形和更高的密度,而HVOF涂层显示出更明显的缺陷和略高的氧化物含量。 Cs涂层和HVOF涂层均导致沉积期间的诱导颗粒的一些损失,而在HVOF复合涂层中达到了较高的诱导颗粒含量,在HVOF沉积期间表明诱导颗粒的较高沉积效率。根据XRD分析,SMC涂层两种涂层在沉积过程中没有明显的氧化和相变。 EDS分析在HVOF沉积期间经过部分熔化的颗粒。摩擦学检测显示CS涂层的更好磨损性能,导致增强的塑性变形和微硬度。 HVOF涂层显示出更好的磁性性能,与Cs涂层相比,矫顽力较低和更高的饱和磁化强度。这可以通过在HVOF沉积期间的诱导颗粒和较小的应变应力产生来解释。

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