Methanesulfinylation of Benzyl Halides with Dimethyl Sulfoxide

Fu Duo; Dong Jun; Du Hongguang; Xuo Jiaxi

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Methanesulfinylation of Benzyl Halides with Dimethyl Sulfoxide

机译：苄基卤化物与二甲基亚砜的甲磺酰化

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A phenyltrimethylammonium tribromide-mediated nucleophilic substitution/oxygen transformation reaction of benzyl halides with DMSO has been developed. In this transition-metal-free reaction, DMSO acts as not only a solvent but also a "S(O)Me" source, thus providing a convenient method for the efficient and direct synthesis of various benzyl methyl sulfoxides.

机译：已经开发出苯基三甲基铵介导的苄基卤化物与DMSO的苄基卤化物的亲核取代/氧转化反应。在这种过渡无金属反应中，DMSO不仅作用于溶剂，而且仅作用于“S（O）ME”的源，从而提供了一种方便的方法，用于高效和直接合成各种苄基甲基亚砜。

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《The Journal of Organic Chemistry》 |2020年第4期|共7页
作者
Fu Duo; Dong Jun; Du Hongguang; Xuo Jiaxi;
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Beijing Univ Chem Technol State Key Lab Chem Resource Engn Dept Organ Chem Coll Chem Beijing 100029 Peoples R China;

Beijing Univ Chem Technol State Key Lab Chem Resource Engn Dept Organ Chem Coll Chem Beijing 100029 Peoples R China;

Beijing Univ Chem Technol State Key Lab Chem Resource Engn Dept Organ Chem Coll Chem Beijing 100029 Peoples R China;

Beijing Univ Chem Technol State Key Lab Chem Resource Engn Dept Organ Chem Coll Chem Beijing 100029 Peoples R China;

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正文语种 eng
中图分类有机化学;
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1. Methanesulfinylation of Benzyl Halides with Dimethyl Sulfoxide [J] . Fu Duo, Dong Jun, Du Hongguang, The Journal of Organic Chemistry . 2020,第4期

机译：苄基卤化物与二甲基亚砜的甲磺酰化
2. Crystal structure of bis(bis{μ3-3-methyl-3-[(4-nitro-2-oxidobenzylidene)amino]propane-1,3-diolato}tris[chlorido(dimethyl sulfoxide)iron(III)]) dimethyl sulfoxide heptasolvate dihydrate [J] . Chygorin E., Smal Y., Omelchenko I.V. Acta Crystallographica Section E: Crystallographic Communications . 2016,第12期

机译：双（双{μ3-3-甲基-3-[（4-硝基-2-氧化苄叉基）氨基]丙烷-1,3-二醇基}三[氯代（二甲基亚砜）铁（III）]）二甲基亚砜的晶体结构二水七溶剂化物
3. Synthetic, structural and vibrational spectroscopic studies in bismuth(III) halide N,N '-aromatic bidentate base systems. III. Some novel bismuth(III) halide N,N '-bidentate ligand (1 : 1) dimethyl sulfoxide solvates [J] . Bowmaker GA., Lee AM., Skelton BW., Australian Journal of Chemistry: A Journal for the Publication of Original Research in All Branches of Chemistry . 1998,第4期

机译：卤化铋N，N′-芳族双齿碱体系的合成，结构和振动光谱研究。三，一些新颖的卤化铋（III）N，N'-双齿配体（1：1）二甲亚砜溶剂化物
4. Characterization of PEDOT:PSS functionalized by dimethyl sulfoxide and triton X-100 and TiO_2 nanoparticles [C] . Anisa Yaseen, A. Vazquez-Lopez, D. Maestre, European Photovoltaic Solar Energy Conference and Exhibition . 2021

机译：转型的表征：二甲基亚砜和TiO_2纳米粒子官能化的PSS
5. I. SPECTROPHOTOMETRIC STUDIES OF POLYSULFIDES IN DIMETHYL SULFOXIDE. II. ELECTROCHEMICAL AND SPECTROPHOTOMETRIC STUDIES OF MOLYBDENUM(VI), (V), (IV), AND (III) COMPLEXES. III. ELECTROCHEMICAL OXIDATION OF TETRAETHYL AMMONIUM HYDROXIDE IN DIMETHYL SULFOXIDE. [D] . DOUB, WILLIAM HOWARD, JR. 1975

机译：I.分光光度法研究二甲基亚砜中的聚合物。二。钼（VI），（V），（IV）和（III）配合物的电化学和分光光度法研究。三，四乙基氢氧化铵在二甲基亚砜中的电化学氧化。
6. Crystal structure of bis(bis{μ3-3-methyl-3-(4-nitro-2-oxidobenzylidene)aminopropane-13-diolato}trischlorido(dimethyl sulfoxide)iron(III)) dimethyl sulfoxide heptasolvate dihydrate [O] . Eduard Chygorin, Yuri Smal, Irina V. Omelchenko 2016

机译：双（双{μ3-3-甲基-3-（4-硝基-2-氧化苄叉基）氨基丙烷-13-二醇基}三氯代（二甲基亚砜）铁（III））二甲基亚砜的晶体结构二水七溶剂化物
7. Metal Halide and Pseudohalide Complexes in Dimethyl Sulfoxide Solution. VIII. Standard Electrode Potentials in Dimethyl Sulfoxide Solution and Exchange Reactions between Dimethyl Sulfoxide and Water, Involving Metal Ions of Groups 1B and 2B. [O] . Sten Ahrland, Ingmar Persson, P. E. Sørensen, 1980

机译：二甲基亚砜溶液中的金属卤化物和伪卤化物配合物。 VIII。二甲基亚甲醚溶液中的标准电极电位和二甲基亚甲醚和水之间的交换反应，涉及组1b和2b的金属离子。
8. Reactions of 1,1-Dimethyl-2,3-Bis(trimethylsilyl)-1-Silirene and Hexamethylsilirane with Dimethyl Sulfoxide. Insertion of Dimethylsilanone into the Silirene and Silirane Rings. [R] . Seyferth, D., Lim, T. F. O., Duncan, D. P. 1977

机译：1,1-二甲基-2,3-双（三甲基甲硅烷基）-1-硅烷和六甲基硅烷与二甲基亚砜的反应。将二甲基硅烷酮插入silirene和silirane环中。

Methanesulfinylation of Benzyl Halides with Dimethyl Sulfoxide

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