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Effect of Initial Grain Size on Thermal Fatigue Behavior and Changes in Microstructure of Ferritic Stainless Steel

机译:初始粒度对铁素体不锈钢微观结构的热疲劳行为及变化的影响

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摘要

To understand the effect of grain size on the thermal fatigue behavior and dynamic recrystallization during the thermal fatigue process in ferritic stainless steel, interrupted testing of thermal fatigue in the temperature range from 473K (minimum) to 1073K (maximum) with a restriction ratio of 50% was conducted for fine-grained (diameter: 38 mu m) and coarse-grained (diameter: 221 mu m) specimens in a Nb- and Si-added ferritic stainless steel tube. The fine-grained specimen showed a small inelastic strain range during the thermal fatigue process and a longer life than the coarse-grained specimen. Microstructure observation by electron back-scatter diffraction revealed that dynamic recovery and recrystallization occurred during the thermal fatigue process. However, the coarse-grained specimen showed lower nucleus density and retardation of the recrystallization in comparison with the fine-grained specimen. From a supposition of the accumulation of the inelastic strain range during thermal fatigue cycles, the relationship between the accumulation strain and Zener-Hollomon parameter for dynamic recovery and recrystallization almost accorded with previous knowledge on this tendency. In addition, we found that for the steady-state recrystallized grain size in thermal fatigue cycles, there was little initial grain size dependence.
机译:要了解晶粒度在铁素体不锈钢的热疲劳过程中对热疲劳行为和动态重结晶的影响,温度范围内的温度疲劳的中断检测从473k(最小)到1073k(最大)的限制比为50在NB和Si-加入的铁素体不锈钢管中进行细粒(直径:38μm)和粗粒(直径:221μm)标本进行的%。细粒度样本在热疲劳过程中显示出小的无弹性应变范围,并且寿命比粗粒样标本更长。电子背散射衍射的微观结构观察显示在热疲劳过程中发生动态回收和再结晶。然而,与细粒样标本相比,粗粒样标本显示较低的核密度和再结晶的延迟。从绝热期间的绝热范围的假设,累积应变与ZENER-HOLLOMON参数之间的关系,用于动态恢复和再结晶几乎符合先前关于这种趋势的知识。此外,我们发现,对于热疲劳循环中的稳态再结晶晶粒尺寸,初始粒度很小依赖性。

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