首页> 外文期刊>Journal of Agricultural and Food Chemistry >Detection of γ-lrradiated Sesame Seeds before and after Roasting by Analyzing Photostimulated Luminescence, Thermoluminescence, and Electron Spin Resonance
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Detection of γ-lrradiated Sesame Seeds before and after Roasting by Analyzing Photostimulated Luminescence, Thermoluminescence, and Electron Spin Resonance

机译:通过分析光刺激的发光,热发光和电子自旋共振来检测焙烧前后γ-辐照芝麻种子

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Sesame seeds were irradiated using a ~(60)Co irradiator (0-4 kGy) and then roasted (220 °C for 10 min). To identify the irradiation treatment, physical detection methods like photostimulated luminescence (PSL), thermoluminescence (TL), and electron spin resonance (ESR) have been investigated before and after roasting. The photon counts of the irradiated samples (nonroasted and roasted) were higher than those of nonirradiated ones, making it possible to distinguish the two samples. The threshold values of nonroasted and roasted samples increased linearly with the irradiation dose, respectively. The TL for the nonirradiated nonroasted and roasted samples presented a lower peak at about 300 °C, but irradiated samples showed a higher peak at around 150 °C. The areas of TL glow curves were 15 times higher in nonroasted as compared with roasted samples. TL ratio [integrated area of TL1 (the first glow)/TL2 (the second glow)] obtained by the reirradiation step was 0 in nonirradiated samples and more than 0.15 in irradiated samples. The radiation-induced ESR signals originating from cellulose were determined in irradiated samples before and after roasting.
机译:使用〜(60)Co辐照器(0-4 kGy)辐照芝麻,然后烘烤(220°C持续10分钟)。为了确定辐照处理方法,已经研究了焙烧前后的物理检测方法,例如光刺激发光(PSL),热发光(TL)和电子自旋共振(ESR)。辐照样品(未焙烧和焙烧)的光子计数高于未辐照样品的光子计数,从而可以区分这两个样品。非焙烤和焙烤样品的阈值分别随辐照剂量线性增加。未辐照的非焙炒和焙烤样品的TL在约300°C时出现较低的峰,但辐照的样品在150°C时显示较高的峰。与焙烤样品相比,非焙烤中TL发光曲线的面积高15倍。通过再照射步骤获得的TL比[TL1(第一辉光)/ TL2(第二辉光)的积分面积]在未辐照样品中为0,在辐照样品中大于0.15。在烘烤之前和之后,在辐照样品中确定源自纤维素的辐射诱发的ESR信号。

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