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Investigating the microstructure and mechanical behaviors of DLC films on AISI52100 bearing steel surface fabricated by plasma immersion ion implantation and deposition

机译:研究等离子浸没离子注入和沉积在AISI52100轴承钢表面上DLC膜的微观结构和力学行为

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摘要

The microstructure and mechanical properties of diamond-like carbon (DLC) films fabricated on an AISI52100 bearing steel substrate surface by plasma immersion ion implantation and deposition (PIIID) were studied. Atomic force microscope (AFM) observation reveals that the DLC film has an extremely smooth surface, and high uniformity and efficiency of space filling over large areas. Raman spectroscopy analysis indicates that DLC films are mainly constituted by amorphous and crystalline phases, with a variable ratio of sp~2/sp~3 carbon bonds, and sp~3 bond content of more than 10%. The maximum nanohardness and elastic modulus of the DLC film are 40GPa and 430GPa, and increase by 263.6% and 95.5%, respectively. The friction and wear results exhibit that the friction coefficient against an AISI52100 steel ball decreases from 0.87 to 0.20. The corrosion polarization curves in a 3.5% saturated NaCl solution shows that the corrosion resistance of DLC/AISI52100 samples is much better than that of bearing steel substrate. Compared with the bare bearing steel, the surface mechanical property of the DLC/AISI52100 sample is improved significantly.
机译:研究了通过等离子体浸没离子注入和沉积(PIIID)在AISI52100轴承钢基底表面上制备的类金刚石碳(DLC)膜的微观结构和力学性能。原子力显微镜(AFM)的观察表明,DLC膜具有极其光滑的表面,并且在大面积上具有很高的均匀性和空间填充效率。拉曼光谱分析表明,DLC薄膜主要由非晶相和结晶相组成,其sp〜2 / sp〜3碳键的比例可变,sp〜3键的含量大于10%。 DLC薄膜的最大纳米硬度和弹性模量分别为40GPa和430GPa,分别增加了263.6%和95.5%。摩擦磨损结果表明,对AISI52100钢球的摩擦系数从0.87降低至0.20。在3.5%NaCl饱和溶液中的腐蚀极化曲线表明,DLC / AISI52100样品的耐蚀性比轴承钢基材的耐蚀性好得多。与裸轴承钢相比,DLC / AISI52100样品的表面力学性能得到了显着改善。

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