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Quantification of probe-sample interactions of a scanning thermal microscope using a nanofabricated calibration sample having programmable size

机译:使用具有可编程大小的纳米级校准样品对扫描热显微镜的探针-样品相互作用进行定量

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摘要

We report a method for quantifying scanning thermal microscopy (SThM) probe-sample thermal interactions in air using a novel temperature calibration device. This new device has been designed, fabricated and characterised using SThM to provide an accurate and spatially variable temperature distribution that can be used as a temperature reference due to its unique design. The device was characterised by means of a microfabricated SThM probe operating in passive mode. This data was interpreted using a heat transfer model, built to describe the thermal interactions during a SThM thermal scan. This permitted the thermal contact resistance between the SThM tip and the device to be determined as 8.33 x 10(5)KW(-1). It also permitted the probe-sample contact radius to be clarified as being the same size as the probe's tip radius of curvature. Finally, the data were used in the construction of a lumped-system steady state model for the SThM probe and its potential applications were addressed.
机译:我们报告了一种使用新型温度校准装置对空气中的扫描热显微镜(SThM)探针-样品热相互作用进行定量的方法。这款新设备已使用SThM设计,制造和表征,以提供准确且空间可变的温度分布,由于其独特的设计而可用作温度参考。该设备的特点是通过在被动模式下运行的微型SThM探针进行表征。使用传热模型解释该数据,该模型用于描述SThM热扫描期间的热相互作用。这样可以确定SThM尖端与设备之间的热接触电阻为8.33 x 10(5)KW(-1)。它还允许将探针-样品的接触半径澄清为与探针的尖端曲率半径相同的大小。最后,将数据用于SThM探针的集总系统稳态模型的构建,并探讨了其潜在应用。

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