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Mechanical and electrical properties of carbon nanofibers reinforced aluminum nitride composites prepared by plasma activated sintering

机译:等离子体活化烧结制备碳纳米纤维增强氮化铝复合材料的力学和电性能

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摘要

High density carbon nanofibers (CNFs) reinforced aluminum nitride (A1N) composites were successfully fabricated by plasma activated sintering (PAS) method. The effects of CNFs on the microstructure, mechanical and electrical properties of the A1N composites were investigated. The experimental results showed that the grain growth of A1N was significantly inhibited by the CNFs. With 2 wt.% CNFs added into the composites, the fracture toughness and flexural strength were increased, respectively to 5.03 MPa m~(1/2) and 354 MPa, which were 20.9% and 13.4% higher than those of monolithic A1N. The main toughening mechanisms were CNFs pullout and bridging, and the main reason for the improvements in strength should be the fine-grain-size effect caused by the CNFs. The DC conductivity of the composites was effectively enhanced through the addition of CNFs, and showed a typical percolation behavior with a very low percolation threshold at the CNFs content of about 0.93 wt.% (1.51 vol.%).
机译:通过等离子活化烧结(PAS)方法成功制备了高密度碳纳米纤维(CNFs)增强氮化铝(AlN)复合材料。研究了CNFs对AlN复合材料的微观结构,力学和电学性能的影响。实验结果表明,CNFs明显抑制了AlN的晶粒长大。在复合物中加入2 wt%的CNF后,断裂韧性和弯曲强度分别提高到5.03 MPa m〜(1/2)和354 MPa,比整体式AlN分别高20.9%和13.4%。主要的增韧机制是CNF的拔出和桥接,强度提高的主要原因应该是CNF引起的细粒度效应。通过添加CNFs可以有效地提高复合材料的DC电导率,并且在CNFs含量约为0.93 wt。%(1.51 vol。%)时表现出典型的渗透行为,并且具有非常低的渗透阈值。

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