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首页> 外文期刊>Journal of industrial and engineering chemistry >A sonochemical-assisted method for synthesis of BaFe_(12)O_(19) nanoparticles and hard magnetic nanocomposites
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A sonochemical-assisted method for synthesis of BaFe_(12)O_(19) nanoparticles and hard magnetic nanocomposites

机译:声化学辅助合成BaFe_(12)O_(19)纳米粒子和硬磁纳米复合材料的方法

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摘要

Hard magnetic BaFe_(12)O_(19) (BaFe) nanoparticles were synthesized via a facile sonochemical-assisted reaction. BaFe nanoparticles were then added to acrylonitrile-butadiene-styrene (ABS) and cellulose acetate (CA) in order to make magnetic nanocomposites. Nanoparticles and nanocomposites were then characterized using X-ray diffraction, scanning electron microscopy and Fourier transform infrared spectroscopy. The magnetic properties of the samples were also investigated using an alternating gradient force magnetometer. The barium ferrite nanoparticles exhibit ferrimagnetic behaviour at room temperature, with a saturation magnetization of 53 emu/g and a coercivity of 2430 Oe. Distribution of the BaFe_(12)O_(19) nanoparticles into the polymeric matrixes increases the coercivity dramatically.
机译:硬磁BaFe_(12)O_(19)(BaFe)纳米粒子是通过便捷的声化学辅助反应合成的。然后将BaFe纳米粒子添加到丙烯腈-丁二烯-苯乙烯(ABS)和醋酸纤维素(CA)中,以制备磁性纳米复合材料。然后使用X射线衍射,扫描电子显微镜和傅里叶变换红外光谱对纳米颗粒和纳米复合材料进行表征。还使用交变梯度力磁力计研究了样品的磁性。钡铁氧体纳米颗粒在室温下表现出亚铁磁性,饱和磁化强度为53 emu / g,矫顽力为2430 Oe。 BaFe_(12)O_(19)纳米粒子分布到聚合物基体中可显着提高矫顽力。

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