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GC-MS investigation of the aroma compounds of Hungarian red paprika (Capsicum annuum) cultivars

机译:匈牙利红辣椒品种香气成分的GC-MS研究

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摘要

Simultaneous distillation-extraction method has been developed for the GC-MS measurement of ground red paprika volatile compounds. The applied benzenemethanol internal standard ensures precise control and determination of the preparation efficiency. MS identification discovered characteristic differences among sweet and hot cultivars. By measuring the Programmed Temperature Retention Indices (PTRI) (after having added) four appropriate hydrocarbons before chromatography) of the components and normalizing the peak areas to one of the most intense chromatographic peaks (methylhexadecanoate), the absolute chromatograms turn into relative "aroma spectra". The run by run PTRI determination and peak area normalization resulted in nearly distortion-free measurement of the compound ratios that are much more characteristic of the aroma patterns than the absolute amounts themselves.
机译:已开发了同时蒸馏-萃取方法用于GC-MS测定地面红辣椒粉挥发性化合物的方法。所应用的苯甲醇内标可确保精确控制和确定制备效率。 MS鉴定发现甜和热品种之间的特征差异。通过测量组分的程序升温保留指数(PTRI)(在色谱分离前添加四种合适的烃类)并将峰面积归一化为最强的色谱峰之一(十六酸甲酯),绝对色谱图就变成了相对的“芳香光谱” ”。通过逐次PTRI测定和峰面积归一化,可以对化合物比率进行几乎无失真的测量,这比绝对量本身具有更多香气特征。

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