Optical Resolution of 2-Azabicyclo[2.2.1]Hept-5-EN-3-One by Inclusion Complexation With Brucine

Koichi Tanaka; Masako Kato; Fumio Toda

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Optical Resolution of 2-Azabicyclo[2.2.1]Hept-5-EN-3-One by Inclusion Complexation With Brucine

机译：Brucine包合物络合的2-氮杂双环[2.2.1] Hept-5-EN-3-One的旋光拆分

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摘要

A simple optical resolution method of 2-azabicyclo[2.2.1]hept-5-en-3-one by inclusion complexation with brucine was reported. The crystal structure of the inclusion complex was analyzed by X-Ray diffraction in order to elucidate the mechanism of the efficient chiral recognition in the inclusion crystals.

机译：报道了一种通过与苯丙氨酸包合络合的2-氮杂双环[2.2.1]庚-5-烯-3-酮的简单光学拆分方法。通过X射线衍射分析包合物的晶体结构，以阐明包合物晶体中有效手性识别的机理。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry 》 |2001年第1期| 共6页
作者
Koichi Tanaka; Masako Kato; Fumio Toda;
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1. Optical Resolution of 2-Azabicyclo[2.2.1]Hept-5-EN-3-One by Inclusion Complexation With Brucine [J] . Koichi Tanaka, Masako Kato, Fumio Toda Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2001 ,第1期

机译：Brucine包合物络合的2-氮杂双环[2.2.1] Hept-5-EN-3-One的旋光拆分
2. Oscillating Crystallization of (+) and (-) Enantiomers during Resolution by Entrainment of 2-Azabicyclo [2.2.1] hept-5-en-3-one [J] . Gerard A. Potter, Chantal Garcia, Raymond McCague, Angewandte Chemie . 1996 ,第15期

机译：通过分离2-氮杂双环[2.2.1] hept-5-en-3-one引起的（+）和（-）对映异构体的振荡结晶。
3. Enzymatic preparation of optically pure (+)-2-azabicyclo[2.2.1]hept-5-en-3-one by (-)-γ-lactamase from Bradyrhizobium japonicum USDA 6 [J] . ZhuS., RenL., YuS., Bioorganic and Medicinal Chemistry Letters . 2014 ,第20期

机译：日本根瘤菌（USDA）的（-）-γ-内酰胺酶酶法制备光学纯的（+）-2-氮杂双环[2.2.1] hept-5-en-3-one 6
4. Applications of fluid inclusion technologies to resolution of complex reservoir exploration and development issues [C] . International symposium on Chinese petroleum exploration in 21st century . 2002

机译：流体包裹体技术在解决复杂油藏勘探开发问题中的应用
5. Calorimetric investigations of enthalpically driven cyclophane-arene inclusion complexation in water, and, Design, synthesis, and binding studies of an optically active ditopic binaphthyl receptor. [D] . Wyman, Tara Buckley. 1993

机译：焓驱动水中的环烷-芳烃夹杂物络合物的量热研究，以及光学活性双位双萘基受体的设计，合成和结合研究。
6. Optical sensor for berberine utilizing its intrinsic fluorescence enhanced by the formation of inclusion complex with butylated-β-cyclodextrin [O] . Yu Yang, Xin Yang, Chen-Xu Jiao, -1

机译：小碱的光学传感器利用其固有荧光可与丁基化β-环糊精形成包合物
7. NOVEL 1,2- AND 1,3-DOUBLE CHIRAL RECOGNITIONS. OPTICAL RESOLUTION OF α- AND β-HALOACETYLENIC ALCOHOLS BY COMPLEXATION WITH BRUCINE [O] . TODA Fumio, TANAKA Koichi, MORI Koji 1983

机译：新颖的1,2-和1,3-双手性识别。芥氨酸配合物光学拆分α-和β-卤代乙炔醇

Optical Resolution of 2-Azabicyclo[2.2.1]Hept-5-EN-3-One by Inclusion Complexation With Brucine

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