SYNTHESIS OF 3-SUBSTITUTED 3-(TRIMETHYLSILOXY)PYRROLIDINES FROM β-AMINOKETONES AND LITHIUM TRIMETHYLSILYLDIAZOMETHANE

Yoshiyuki Hari; Takuya Yokoyama; Toyohiko Aoyama

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SYNTHESIS OF 3-SUBSTITUTED 3-(TRIMETHYLSILOXY)PYRROLIDINES FROM β-AMINOKETONES AND LITHIUM TRIMETHYLSILYLDIAZOMETHANE

机译：由β-酰胺基酮和三甲基三甲基甲硅烷基重氮甲基锂合成3-取代的3-（三甲基甲氧基）吡咯烷酮

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Lithium trimethylsilyldiazomethane reacted with N-benzyl-β-aminoketones at-78 °C in THF to give 3-substituted 1-benzyl-3-(trimethylsiloxy)pyrrolidines in moderate to good yields.

机译：三甲基硅烷基重氮甲烷锂与N-苄基-β-氨基酮在THF中于-78°C反应，以中等至良好的收率得到3-取代的1-苄基-3-（三甲基甲硅烷氧基）吡咯烷。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2010年第1期|共9页
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Yoshiyuki Hari; Takuya Yokoyama; Toyohiko Aoyama;
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1. SYNTHESIS OF 3-SUBSTITUTED 3-(TRIMETHYLSILOXY)PYRROLIDINES FROM β-AMINOKETONES AND LITHIUM TRIMETHYLSILYLDIAZOMETHANE [J] . Yoshiyuki Hari, Takuya Yokoyama, Toyohiko Aoyama Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2010,第1期

机译：由β-酰胺基酮和三甲基三甲基甲硅烷基重氮甲基锂合成3-取代的3-（三甲基甲氧基）吡咯烷酮
2. New synthesis of 3-substituted indoles using lithium trimethylsilyldiazomethane [J] . Takashi Miyagi, Yoshiyuki Hari, Toyohiko Aoyama Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2004,第33期

机译：三甲基甲硅烷基重氮甲烷锂新合成3-取代的吲哚
3. Using heteroaryl-lithium reagents as hydroxycarbonyl anion equivalents in conjugate addition reactions with (S, S)-(+)-pseudoephedrine as chiral auxiliary; Enantioselective synthesis of 3-substituted pyrrolidines [J] . Alonso B., Ocejo M., Carrillo L., The Journal of Organic Chemistry . 2013,第2期

机译：在（S，S）-（+）-伪麻黄碱作为手性助剂的共轭加成反应中，使用杂芳基-锂试剂作为羟羰基阴离子当量; 3-取代的吡咯烷的对映选择性合成
4. Synthesis, Characterization and bulk crystal growth of nonlinear 3-substituted salicylidene aniline derivatives [C] . K. Bhat, T. Gebre, A. K. Batra, Conference on Linear and Nonlinear Optics of Organic Materials III; Aug 4-6, 2003; San Diego, California, USA . 2003

机译：非线性3-取代水杨基苯胺衍生物的合成，表征和体相生长
5. The Synthesis of α-Aminoketones via Titanium Promoted Cross Electrophile Coupling of Imines with Weinreb Amides [D] . Alkhamayseh, Osaid. 2021

机译：通过钛的α-氨基酮的合成促进亚胺的杂交电泳偶联与Weinreb酰胺
6. Synthesis of 3-Substituted Pyrrolidines via Palladium-Catalyzed Hydroarylation [O] . Joseph B. Sweeney, Julien Doulcet, Bimod Thapa 2018

机译：钯催化的氢芳基化反应合成3-取代的吡咯烷
7. New methods and reagents in organic synthesis. 31. Lithium trimethylsilyldiazomethane: A new synthon for the preparation of tetrazoles. [O] . Toyohiko Aoyama, Takayuki Shioiri 1982

机译：有机合成中的新方法和试剂。 31.锂三甲基甲基甲硅烷二甲基甲烷：一种用于制备四唑的新合成。

SYNTHESIS OF 3-SUBSTITUTED 3-(TRIMETHYLSILOXY)PYRROLIDINES FROM β-AMINOKETONES AND LITHIUM TRIMETHYLSILYLDIAZOMETHANE

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