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首页> 外文期刊>Zeitschrift fur Physikalische Chemie: International Journal of Research in Physical Chemistry and Chemical Physics >Low Energy Electron Point Source Microscopy of Two-Dimensional Carbon Nanostructures
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Low Energy Electron Point Source Microscopy of Two-Dimensional Carbon Nanostructures

机译:二维碳纳米结构的低能电子点源显微镜

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摘要

1 nm thick carbon nanomembranes (CNMs) are investigated with Low Energy Electron Point Source (LEEPS) microscopy. A CNM consists of a freely suspended carbon film made from a cross-linked self-assembled monolayer (SAM). During thermal annealing the CNM transforms into nanocrystalline graphene. We determined the electron transmissivity of CNMs from the LEEPS images. After pyrolysis, the LEEPS images showed clear differences compared to pristine CNMs. Upon annealing above 800 °C the LEEPS images exhibit distinct features that are related to the structural transition. A comparison of LEEPS images with transmission electron micrographs of the same regions and features demonstrates that both microscopic techniques reveal similar structural features.
机译:用低能量电子点源(LEEPS)显微镜研究了1 nm厚的碳纳米膜(CNMs)。 CNM由由交联的自组装单层(SAM)制成的自由悬浮的碳膜组成。在热退火过程中,CNM转变为纳米晶石墨烯。我们从LEEPS图像中确定了CNM的电子透射率。热解后,LEEPS图像与原始CNM相比显示出明显的差异。在800°C以上退火时,LEEPS图像显示出与结构转变有关的独特特征。 LEEPS图像与相同区域和特征的透射电子显微照片的比较表明,两种显微技术均显示出相似的结构特征。

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