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Nano/microtribology stick-slip number under an atomic force microscope and its characteristics

机译:原子力显微镜下的纳米/微摩擦学粘滑数及其特性

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The atomic force microscope (AFM) has become a main instrument in observing nano/microtribological characteristics of sample surfaces. In this paper, we investigated the micro-scale adhesive contact between the AFM tip and the sample surface based on the Maugis-Dugdale contact model, and analyzed the energy conversion and dissipation process during the AFM scanning process. A dimensionless stick-slip number η = {the square root of}(8U{sub}1h{sup}2/(k{sub}θ(R{sub}s){sup}2)) was defined, which can serve as a characteristic index for the appearance of nano/microtribology stick-slip behavior. If the stick-slip number is less than one, i.e., η < 1, the AFM tip slides on the sample surface and no stick-slip behavior occurs in the AFM lateral force signal. When the stick-slip number equals one, i.e., η= 1, the tip jumps on the sample surface and the AFM lateral force signal begins to exhibit a stick-slip behavior but without energy dissipation. Only in the case ofη> 1 does the stick-slip behavior appear in the AFM lateral force signal accompanied by an obvious energy dissipation. The defined stick-slip number demonstrates that the nano/microtribological stick-slip behavior is due to the adhesive hysteresis as well as the instability motion of the AFM tip during the scanning process. Finally, the influence on nano/microtribology stick-slip behavior of sample surface energy, surface topography, scanning velocity, spring constant of AFM cantilever probe, etc. are investigated theoretically and experimentally. Various experimental results of nano/microtribology stick-slip behavior under AFM are successfully interpreted according to the stick-slip number.
机译:原子力显微镜(AFM)已成为观察样品表面纳米/微生物学特征的主要工具。在本文中,我们基于Maugis-Dugdale接触模型研究了AFM尖端与样品表面之间的微型粘合剂接触,并分析了AFM扫描过程中的能量转换和耗散过程。定义了无量纲粘滑数η= {}(8U {sub} 1h {sup} 2 /(k {sub}θ(R {sub} s){sup} 2))的平方根作为纳米/微摩擦学粘滑行为外观的特征指标。如果粘滑数小于1,即η<1,则AFM尖端会在样品表面上滑动,并且AFM横向力信号中不会发生粘滑行为。当粘滑数等于1,即η= 1时,尖端在样品表面上跳动,AFM横向力信号开始表现出粘滑行为,但没有能量消耗。仅在η> 1的情况下,粘滑行为才会出现在AFM横向力信号中,并伴有明显的能量耗散。定义的粘滑数表明,纳米/微生物摩擦粘滑行为是由于胶粘剂滞后以及AFM尖端在扫描过程中的不稳定性而引起的。最后,从理论上和实验上研究了样品表面能,表面形貌,扫描速度,AFM悬臂探针的弹簧常数等对纳米/微摩擦学粘滑行为的影响。根据粘滑数成功地解释了纳米/微生物摩擦学在AFM下粘滑行为的各种实验结果。

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