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Dry-Blasting of α- and κ-Al_2O_3 CVD Hard Coatings: Friction Behaviour and Thermal Stress Relaxation

机译:干炸α-和κ-Al_2O_3CVD硬质涂层的摩擦行为和热应力松弛

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摘要

Post-deposition blasting treatments of cemented carbide cutting tools coated by chemical vapour deposition have gained increasing interest. Within the present work, α- and κ-Al_2O_3 coatings dry-blasted using different pressures as well as globular and edged blasting materials were investigated. A higher pressure resulted in an increase in the compressive residual stresses, as determined by X-ray diffraction. Both blasting materials had a minor influence on the roughness of α-Al_2O_3, while the edged material caused a significant roughness increase for κ-Al_2O_3. For α-Al_2O_3 dry-blasted using the globular material, complete stress relaxation could be observed after annealing at 500℃, whereas for α-Al_2O_3 dry-blasted using the edged material as well as for the κ-Al_2O_3, an annealing temperature of 900℃ was necessary for stress relaxation. The friction coefficient of the dry-blasted samples first increases with increasing temperature, due to increasing plastic deformation of the blasting material transferred onto the coating surface, until it decreases again above 700℃, due to softening of the transferred material.
机译:通过化学气相沉积涂覆的硬质合金刀具的沉积后喷砂处理引起了越来越多的关注。在目前的工作中,研究了使用不同压力进行干喷的α-和κ-Al_2O_3涂层以及球状和边缘式喷砂材料。较高的压力导致了压缩残余应力的增加,这是通过X射线衍射确定的。两种喷砂材料对α-Al_2O_3的粗糙度影响均较小,而磨边材料则导致κ-Al_2O_3的粗糙度显着增加。使用球状材料进行干喷处理的α-Al_2O_3,在500℃退火后可以观察到完全的应力松弛,而对于使用刃状材料进行干喷处理的α-Al_2O_3以及使用κ-Al_2O_3进行喷丸处理的退火温度为900 ℃对于应力松弛是必要的。干喷丸样品的摩擦系数首先随着温度的升高而增加,这是由于传递到涂层表面的喷砂材料的塑性变形增加,直到由于转移材料的软化而再次降低到700℃以上。

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