Observation of a new dimeric amino acid derivative in the reaction of methyl N-BOC-(S)-(3-fluorophenyl)alanate with DIBAL-H and lithio ethyl propiolate

Jasys VJ.; Urban FJ.

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Observation of a new dimeric amino acid derivative in the reaction of methyl N-BOC-(S)-(3-fluorophenyl)alanate with DIBAL-H and lithio ethyl propiolate

机译：N-BOC-（S）-（3-氟苯基）丙氨酸甲酯与DIBAL-H和硫代丙酸乙硫酯反应中新的二聚氨基酸衍生物的观察

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A novel amino acid dimer 9a was isolated while trying to apply a known reductionucleophilic addition sequence. This dimer provided information both on the mechanism of the process and on the dependence of the desired reaction on the stoichiometry of reagents. (C) 2001 Elsevier Science Ltd. All rights reserved. [References: 7]

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《Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry》 |2001年第3期|共3页
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Jasys VJ.; Urban FJ.;
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1. Observation of a new dimeric amino acid derivative in the reaction of methyl N-BOC-(S)-(3-fluorophenyl)alanate with DIBAL-H and lithio ethyl propiolate [J] . Jasys VJ., Urban FJ. Tetrahedron, Asymmetry: The International Journal for Repid Publication on all Aspects of Asymmetry in Orgainc, Inorganic, Organometallic, Physical and Bio-Organic Chemistry . 2001,第3期

机译：N-BOC-（S）-（3-氟苯基）丙氨酸甲酯与DIBAL-H和硫代丙酸乙硫酯反应中新的二聚氨基酸衍生物的观察
2. Samarium (II) iodide-induced intermolecular coupling of α,β-unsaturated esters with ketones: reactions of methyl propiolate and ethyl buta-2,3-dienoate with cyclohexanone and its application to synthesis of a terpene carboxylic acid [J] . Masakazu Sono, Natsuki Doi, Eri Yoshino Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2013,第15期

机译：碘化mar（II）诱导的α，β-不饱和酯与酮的分子间偶联：丙酸甲酯和2,3-丁二酸乙基酯与环己酮的反应及其在合成萜烯羧酸中的应用
3. Reaction of magnesium carbenoids with N-lithio arylamines:a novel method for generation of non-stabilized alpha-amino-substituted carbanions and a new synthesis of alpha-amino acid derivatives [J] . Tsuyoshi Satoh, Atsushi Osawa, Atsushi Kondo Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2004,第36期

机译：镁类胡萝卜素与N-硫代芳基胺的反应：生成不稳定的α-氨基取代的碳负离子的新方法和α-氨基酸衍生物的新合成
4. Transition Structure Models of Organic Reactions in Chloroaluminate Ionic Liquids: Cyclopentadiene and Methyl Acrylate Diels-Alder Reaction in Acidic and Basic Melts of 1-Ethyl-3-methylimidazolium Chloride with Aluminum(Ⅲ) Chloride [C] . Orlando Acevedo, Jeffrey D. Evanseck, American Chemical Society, Symposium ionic liquids as green solvents: Progress and prospects . 2003

机译：氯铝酸铝离子液体有机反应的过渡结构模型：氯化铝（Ⅲ）氯化铝酸性和碱性熔体中的环戊二烯和丙烯酸甲基丙烯酸甲基丙烯酸甲酯反应
5. Asymmetric Mannich reactions catalyzed by urea derivatives for the enantioselective preparation of beta-aryl-beta-amino acid derivatives. [D] . Wenzel, Anna G. 2004

机译：由脲衍生物催化的不对称曼尼希反应用于对映选择性制备β-芳基-β-氨基酸衍生物。
6. Crystal structures of two stilbazole derivatives: bis{(E)-4-4-(diethylamino)styryl-1-methylpyridin-1-ium} tetraiodidocadmium(II) and (E)-4-4-(diethylamino)styryl-1-methylpyridin-1-ium 4-methoxybenzenesulfonate monohydrate [O] . Priya Antony, S. Antony Inglebert, Jerald V. Ramaclus, 2018

机译：两种stilbazole衍生物的晶体结构：双{（E）-4- 4-（二乙基氨基）苯乙烯基 -1-甲基吡啶-1-基}四碘镉镉（II）和（E）-4- 4-（二乙基氨基）苯乙烯基 -1-甲基吡啶-1-4-甲氧基苯磺酸一水合物
7. Influence of Lewis Acids on the Diels–Alder Reaction. VII. The Reaction of Furan with Ethyl Propiolate [O] . A. W. McCulloch, D. G. Smith, A. G. McInnes 1974

机译：路易斯酸对Diels-ald反应的影响。 VII。呋喃与乙酸乙酯的反应

Observation of a new dimeric amino acid derivative in the reaction of methyl N-BOC-(S)-(3-fluorophenyl)alanate with DIBAL-H and lithio ethyl propiolate

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