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Fabrication and magnetic properties of Sm-Co/Fe-Co and Sm-Co/Fe-Co-Dy magnetic nanowires

机译:Sm-Co / Fe-Co和Sm-Co / Fe-Co-Dy磁性纳米线的制备及磁性

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The Sm-Co/Fe-Co and Sm-Co/Fe-Co-Dy nanowire arrays with smaller diameter are prepared by electrochemical deposition on the anodic aluminum oxide (AAO) templates in this paper. The crystal structure and magnetic properties of nanowires are characterized and analyzed. It is found that the Sm-Co nanowires change from amorphous phase to nanocrystalline state with hard magnetic characterization through annealing at 660 ℃ for 3 h. In this experiment, rare earth element Dy is added to the Fe-Co solution, and the three alloy nanowires are prepared and researched for the first time. The addition of Dy element produces a new Fe_(23)Dy_6 phase in the nanowires. The magnetic hysteresis loops illustrate that the magnetic properties of as-deposited nanowires is improved dramatically after heat treatment and the direction parallel to the nanowire arrays is the easy direction of magnetization which leads to nanowires possessing obvious shape anisotropy. The effect of different Dy ion concentration on nanowires' magnetic properties is investigated in this paper.
机译:通过在阳极氧化铝(AAO)模板上进行电化学沉积,制备了直径较小的Sm-Co / Fe-Co和Sm-Co / Fe-Co-Dy纳米线阵列。对纳米线的晶体结构和磁性进行了表征和分析。通过660℃退火3 h,发现Sm-Co纳米线由非晶态转变为纳米晶,具有硬磁特性。在该实验中,将稀土元素Dy添加到Fe-Co溶液中,首次制备和研究了三种合金纳米线。 Dy元素的添加在纳米线中产生新的Fe_(23)Dy_6相。磁滞回线表明,热处理后,沉积态纳米线的磁性能得到显着改善,并且平行于纳米线阵列的方向是容易磁化的方向,这导致纳米线具有明显的形状各向异性。本文研究了不同Dy离子浓度对纳米线磁性能的影响。

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  • 来源
    《Superlattices and microstructures》 |2017年第7期|246-253|共8页
  • 作者单位

    Key Lab. for New Type of Functional Materials in Hebei Province, School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130, China;

    Key Lab. for New Type of Functional Materials in Hebei Province, School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130, China;

    Key Lab. for New Type of Functional Materials in Hebei Province, School of Materials Science and Engineering, Hebei University of Technology, No. 8, Road No. 1, Dingzigu, Hongqiao District, Tianjin 300130, China;

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