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Evaluation of Parameters Influencing Hexavalent Chromium Mist Sampling: A Full Factorial Design

机译:影响六价铬雾采样参数的评估:全因子设计

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A chromium electroplating bath with the ability to produce homogenous mist was used to evaluate parameters influencing hexavalent chromium (Cr~(+6)) mist sampling methods. The results of 48 Cr~(+6) mist samples collected using the U.S. National Institute for Occupational Safety and Health method 7600 showed that Cr~(+6) concentration was higher: (1) For sampling by closed-face filter cassettes than for sampling by open-face filter cassettes (P < 0.001); (2) for samples collected at 35 cm above the electroplating solution surface than for samples collected at 50 cm (P <0.001); (3) for sampling duration of 30 minutes than for sampling duration of 180 minutes (P <0.001); and, (4) for samples extracted immediately after sampling than for samples with delayed extraction (24 hours after sampling) (P<0.001). It is concluded that the accuracy of Cr~(+6) mist sampling in electroplating shops will be enhanced when: (1) closed-face filter cassette is used to prevent liquid splash contamination; (2) the recommended sampling height is 35 cm above the solution surface; (3) the sampling duration is short-approximately 30 minutes; and, (4) the extraction of the Cr~(+6) sample is performed as soon as the sampling is completed.
机译:使用能够产生均质雾的铬电镀液来评估影响六价铬(Cr〜(+6))雾取样方法的参数。使用美国国家职业安全与卫生研究所7600方法收集的48个Cr〜(+6)薄雾样品的结果表明,Cr〜(+6)浓度较高:(1)对于封闭式滤盒而言,Cr〜(+6)比用敞开式滤盒取样(P <0.001); (2)在电镀液表面上方35 cm处采集的样品要比在50 cm处采集的样品要好(P <0.001); (3)30分钟的采样时间比180分钟的采样时间(P <0.001); (4)采样后立即提取的样品比延迟提取样品(采样后24小时)要高(P <0.001)。可以得出结论,在以下情况下,可以提高电镀车间Cr〜(+6)薄雾采样的准确性:(1)使用封闭式滤盒防止液体飞溅物污染; (2)建议的采样高度为溶液表面以上35厘米; (3)采样时间短约30分钟; (4)采样完成后立即进行Cr〜(+6)样品的提取。

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