首页> 外文期刊>International journal of environmental analytical chemistry >Hydrothermal synthesis of nitrogen-doped carbon dots as a sensitive fluorescent probe for the rapid, selective determination of Hg~(2+)
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Hydrothermal synthesis of nitrogen-doped carbon dots as a sensitive fluorescent probe for the rapid, selective determination of Hg~(2+)

机译:氮掺杂碳点的水热合成作为灵敏的荧光探针,用于快速,选择性地测定Hg〜(2+)

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摘要

In the present work, a green synthetic method for producing nitrogen-doped carbon dots (NCDs) by using ammonium citrate and urea is introduced. The obtained NCDs were characterised by transmission electron microscopy, Fourier transform infrared spectra, UV-vis absorption and fluorescence spectra. The results showed that the prepared NCDs were spherical with a size of about 3.5 nm, emitting strong and stable blue fluorescence when excited at 352 nm. It was noting that the NCDs enable sensitive and selective determination of Hg2+ in tap water with a linear range of 0.01-5 mg L-1 based on a possible charge transfer process. The detection limit was 9.4 mu g L-1.
机译:在当前的工作中,介绍了一种绿色合成方法,该方法通过使用柠檬酸铵和尿素生产氮掺杂碳点(NCD)。通过透射电子显微镜,傅立叶变换红外光谱,UV-vis吸收和荧光光谱对获得的NCD进行表征。结果表明,所制备的NCD为球形,尺寸约为3.5nm,在352nm激发时发出强而稳定的蓝色荧光。值得注意的是,基于可能的电荷转移过程,NCD可以灵敏和选择性地测定线性范围为0.01-5 mg L-1的自来水中Hg2 +。检出限为9.4μgL-1。

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