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METHOD FOR SYNTHESIZING FLUORESCENT NITROGEN-DOPED CARBON QUANTUM DOTS FROM FOOD WASTES

机译:食品中合成氮掺杂的碳量子点的方法

摘要

The present utility model relates to a method for synthesizing fluorescent carbon quantum dots (CQDs) with nitrogen functional groups from food wastes, comprising the steps of: preparing and washing the carbon source material with water, wherein the carbon source material comprises the at least one food waste; drying the washed carbon source material via an oven dryer at about 100 øC; dispersing the dried carbon source material in an acid solution to produce a first solution, wherein the acid solution is a 1 pcnt acid solution and the ratio of the first solution is 1 g dried carbon source material: 12.5 mL acid solution; adding tetraethylenepentamine (TEPA) to the first solution to produce a second solution, wherein TEPA acts as a reactant to incorporate nitrogen functional groups; subjecting the second solution to hydrothermal treatment to produce a third solution containing synthesized CQDs with nitrogen functional groups, wherein the hydrothermal treatment is performed at 180 øC - 220 øC for at least 4 -12 hours via an autoclave chamber; centrifuging the third solution at at least 12,000 rpm via a centrifuge to separate unreacted materials from the synthesized CQDs with nitrogen functional groups; and filtering the centrifuged third solution to obtain the synthesized CQDs with nitrogen function groups in solution. The synthesized fluorescent CQDs with nitrogen functional groups can be used in bioimaging and biosensing applications.
机译:本实用新型涉及一种从餐厨垃圾中合成具有氮官能团的荧光碳量子点的方法,其包括以下步骤:用水制备和洗涤碳源材料,其中碳源材料包括至少一种食物浪费;将经洗涤的碳源材料通过烤箱干燥器在约100℃下干燥;将干燥的碳源材料分散在酸溶液中以产生第一溶液,其中酸溶液为1pnt酸溶液,并且第一溶液的比例为1g干燥的碳源材料:12.5mL酸溶液;向第一溶液中加入四亚乙基五胺(TEPA)以制备第二溶液,其中TEPA充当结合氮官能团的反应物;使第二溶液进行水热处理以产生包含具有氮官能团的合成CQD的第三溶液,其中经由高压釜室在180℃至220℃下进行至少4-12小时的水热处理;通过离心机以至少12,000 rpm的速度离心第三种溶液,以从合成的具有氮官能团的CQD中分离出未反应的物质;过滤第三溶液,得到溶液中具有氮官能团的合成CQD。具有氮官能团的合成荧光CQD可用于生物成像和生物传感应用。

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