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Early stage damage of ultrafine-grained tungsten materials exposed to low energy helium ion irradiation

机译:低能氦离子辐照下超细晶粒钨材料的早期损伤

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摘要

Tungsten is considered as a plasma facing component in the divertor region of the International Thermonuclear Experiment Reactor (ITER). High flux, high fluence helium (He) exposure of tungsten surfaces induces severe morphology changes and nanostructure formation, which may eventually erode tungsten and risk the operation of the reactor. In this study, we investigate the response of ultrafine-grained tungsten under low flux (similar to 10(20) ions m(-2) s(-1)), low fluence, low energy (30-70 eV) He irradiation at different temperatures in order to study the early stage of nanostructure formation. Rod-shape nanostructures formed at low temperatures (600 degrees C) and a He fluence of 1 x 10(23) m(-2). High resolution, cross-section TEM images of irradiated grains demonstrated bubble formation not inside the nanostructures but deep inside the grains. At higher temperatures (900 degrees C) and the same fluence of 1 x 10(23) m(-2), large tungsten asperities (stone-shape and fiber-form structures), which are attributed to the burst and erosion of the surface grains. Moreover, low fluence (10(20) m(-2)-10(21) m(-2)) and high temperature (900 degrees C) irradiation demonstrated low density of non-coalesced bubbles inside the TEM samples. The results suggest that morphology changes can exist in He irradiated tungsten even with low bubble densities; thus, an additional factor such as surface stresses may dictate the observed nanostructure formation. (C) 2015 Elsevier B.V. All rights reserved.
机译:钨被认为是国际热核实验反应堆(ITER)偏滤器区域中面向等离子体的成分。钨表面的高通量,高通量氦气(He)暴露会引起严重的形态变化和纳米结构的形成,最终可能腐蚀钨,并危及反应器的运行。在这项研究中,我们研究了超细晶粒钨在低通量(类似于10(20)离子m(-2)s(-1)),低通量,低能量(30-70 eV)He辐照下的响应以不同的温度研究纳米结构形成的早期阶段。棒状纳米结构在低温(600摄氏度)和1 x 10(23)m(-2)的He能量密度下形成。高分辨率,横截面透射电镜的TEM图像表明,气泡不是在纳米结构内部而是在颗粒内部深处形成。在更高的温度(900摄氏度)和相同的注量1 x 10(23)m(-2)下,钨的粗糙(石头状和纤维状结构),归因于表面的破裂和腐蚀谷物。此外,低通量(10(20)m(-2)-10(21)m(-2))和高温(900摄氏度)辐射表明TEM样品内部的非凝聚气泡密度低。结果表明,即使气泡密度低,He照射的钨中也可能存在形态变化。因此,诸如表面应力之类的附加因素可能决定观察到的纳米结构的形成。 (C)2015 Elsevier B.V.保留所有权利。

著录项

  • 来源
    《Fusion Engineering and Design》 |2015年第4期|9-14|共6页
  • 作者单位

    Purdue Univ, Sch Nucl Engn, W Lafayette, IN 47906 USA|Purdue Univ, Sch Mat Engn, W Lafayette, IN 47906 USA|Purdue Univ, Birck Nanotechnol Ctr, W Lafayette, IN 47906 USA;

    Purdue Univ, Sch Nucl Engn, W Lafayette, IN 47906 USA;

    Purdue Univ, Birck Nanotechnol Ctr, W Lafayette, IN 47906 USA;

    Purdue Univ, Sch Mat Engn, W Lafayette, IN 47906 USA;

    FOM Inst DIFFER Dutch Inst Fundamental Energy Res, NL-3439 MN Nieuwegein, Netherlands;

    FOM Inst DIFFER Dutch Inst Fundamental Energy Res, NL-3439 MN Nieuwegein, Netherlands;

    FOM Inst DIFFER Dutch Inst Fundamental Energy Res, NL-3439 MN Nieuwegein, Netherlands;

    Sandia Natl Labs, Dept Radiat Solid Interact, Albuquerque, NM 87185 USA;

    Purdue Univ, Sch Nucl Engn, W Lafayette, IN 47906 USA|Purdue Univ, Sch Mat Engn, W Lafayette, IN 47906 USA|Purdue Univ, Birck Nanotechnol Ctr, W Lafayette, IN 47906 USA;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    TEM; Irradiation; Tungsten; Fusion; Bubble formation;

    机译:TEM;辐照;钨;融合;气泡形成;

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