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High temperature deformability of ductile flash-sintered ceramics via in-situ compression

机译:韧性快速烧结陶瓷的原位压缩高温变形

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Flash sintering has attracted significant attention as its remarkably rapid densification process at low sintering furnace temperature leads to the retention of fine grains and enhanced dielectric properties. However, high-temperature mechanical behaviors of flash-sintered ceramics remain poorly understood. Here, we present high-temperature (up to 600?°C) in situ compression studies on flash-sintered yttria-stabilized zirconia (YSZ). Below 400?°C, the YSZ exhibits high ultimate compressive strength exceeding 3.5?GPa and high inelastic strain (~8%) due primarily to phase transformation toughening. At higher temperatures, crack nucleation and propagation are significantly retarded, and prominent plasticity arises mainly from dislocation activity. The high dislocation density induced in flash-sintered ceramics may have general implications for improving the plasticity of sintered ceramic materials.
机译:闪速烧结引起了广泛的关注,因为其在低烧结炉温度下的快速致密化过程可保留细晶粒并增强介电性能。然而,对于快速烧结陶瓷的高温机械性能仍然知之甚少。在这里,我们介绍了高温快速烧结氧化钇稳定的氧化锆(YSZ)的原位压缩研究(最高600°C)。低于400°C时,YSZ表现出超过3.5?GPa的高极限抗压强度和主要由于相变增韧而导致的高非弹性应变(约8%)。在较高的温度下,裂纹成核和扩展明显受阻,并且显着的塑性主要来自位错活性。在快速烧结陶瓷中引起的高位错密度可能对提高烧结陶瓷材料的可塑性具有普遍意义。

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