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Simple Precipitation Synthesis of Pure Cu3V2O8 Nanoparticles and Investigation of their Optical Properties

机译:Cu3V2O8纳米粒子的简单沉淀合成及其光学性质的研究

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Copper vanadate nanostructures were prepared via ex-situ precipitation approach in presence of Schiff-base ligand (N,N? -buthylenebis(acetylacetone iminato)dianion = acacbn) as a new capping agent. The effect of different Cu sources and pH on the size, morphology and size distribution of copper vanadate nanostructures was investigated. The as-prepared products were characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), Fourier transform infrared (FT-IR) spectrum, Electron Dispersive X-ray spectroscopy (EDX) and ultraviolet– visible (UV–Vis) spectroscopy. The optical properties of different samples were compared.
机译:钒酸铜纳米结构是通过在作为新的封端剂的席夫碱配体(N,N 2-丁二双(乙酰丙酮亚氨基)二阴离子= acacbn)存在下通过异位沉淀法制备的。研究了不同Cu源和pH值对钒酸铜纳米结构的尺寸,形貌和尺寸分布的影响。使用X射线衍射(XRD),扫描电子显微镜(SEM),傅立叶变换红外(FT-IR)光谱,电子色散X射线光谱(EDX)和紫外可见光谱(UV-Vis)对所制备的产品进行表征)光谱学。比较了不同样品的光学性质。

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