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Determination of plasticizers in drinking water using gas chromatography and mass spectrometry

机译:气相色谱和质谱法测定饮用水中的增塑剂

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This study investigated the levels of plasticizer endocrine disruptors (diethyl phthalate, dibutyl phthalate, and bisphenol A) in drinking water at Paraíba do Sul River region and release of these compounds from bottled water. An analytical method employing solid phase extraction and GC/MS was optimized and validated. The results showed that the method is selective, linear (r2 0.99), precise (RSD 12%), accurate (recoveries between 62 and 105%), sensitive and robust. Applying the method, the presence of all studied pollutants in drinking water was observed for the three sampled plasticizers. These plasticizers were not found in mineral bottled water, before or after storage.
机译:这项研究调查了南帕拉伊巴河地区饮用水中增塑剂内分泌干扰物(邻苯二甲酸二乙酯,邻苯二甲酸二丁酯和双酚A)的水平以及从瓶装水中释放这些化合物的情况。优化并验证了采用固相萃取和GC / MS的分析方法。结果表明,该方法具有选择性,线性(r2> 0.99),精确(RSD <12%),准确(回收​​率在62%和105%之间),灵敏且稳定。应用该方法,对三种采样的增塑剂观察到饮用水中所有研究的污染物的存在。这些增塑剂在储存之前或之后在矿泉水瓶中均未发现。

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