Uso de frascos de polipropileno descartáveis no pré-tratamento de amostras de água para determina??o de chumbo, cobre e mercúrio por voltametria de onda quadrada

摘要

In this work a simple and versatile procedure is described for treating water samples using small polypropylene (PP) vials (4 mL) for determining heavy metals by square wave voltammetry (SWV). This procedure involves treatment with nitric acid (0.2 mol L-1) and boiling in a water-bath (~ 100 oC). This process is completed after one hour and allows the pretreatment of several samples simultaneously. The accuracy was estimated using addition/recovery studies and certified water sample analysis, yielding an agreement near to 100%.