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Determination of benzyl isothiocyanate in Carica papaya using gas chromatography with selectives detectors

机译:选择性检测器气相色谱法测定番木瓜中异硫氰酸苄酯

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In the present work, a method was developed and validated for the quantification of benzyl isothiocyanate (BITC) in the fruits of Carica papaya. The quantification of this compound was carried out by gas chromatography (GC) with selective detectors - nitrogen phosphorus detector (NPD) and flame photometric detector (FPD). The performance of these detectors showed a higher sensitivity of the NPD with a broader linear range of detection. The LOD/LOQ were 0.038/0.100 µg/mL for NPD and 5.78/19.29 µg/mL for FPD. The recovery of the method for BITC was 90,64%. An average value of BITC concentration in all the analyzed samples was 16,23 µg BITC/g.
机译:在目前的工作中,开发了一种方法并验证了番木瓜果实中异硫氰酸苄酯(BITC)的定量方法。通过具有选择检测器的氮色谱检测器(NPD)和火焰光度检测器(FPD)的气相色谱法(GC)进行该化合物的定量。这些检测器的性能表明NPD的灵敏度更高,检测范围更广。 NPD的LOD / LOQ为0.038 / 0.100 µg / mL,FPD的LOD / LOQ为5.78 / 19.29 µg / mL。 BITC方法的回收率为90.64%。所有分析样品中BITC浓度的平均值为16,23 µg BITC / g。

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