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Stability of Nanocomposite Edible Films Based on Polysaccharides and Vitamin C from Agroindustrial Residue

机译:基于农残的多糖和维生素C的纳米复合可食用膜的稳定性

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The agroindustrial residue from the production of acerola pulp is rich in residual vitamin C. Thus, aiming its extraction and stabilization, this work proposed the nanoparticle (NP) encapsulation via ionic gelation with subsequent preparation of nanocomposites (NC) film based on galactomannan matrix. NP were characterized and their stabilities were evaluated under different storage conditions (incidence of light, temperature and oxidizing atmosphere). The results by Dynamic Light Scattering (DLS) and Scanning Electron Microscopy (SEM) indicated homogeneous morphology, spherical shape and size of ~220 nm. Regarding the stability, the UV-visible spectrophotometric analysis showed a much lower degradation rate for encapsulated vitamin C, resulting in more than 30% of preservation compared with the non-encapsulated systems at the end of 15th day of storage. In agreement, the NC films also resulted in preservation of vitamin C mainly for the test in high temperature, which maintained about 80% of the initial concentration, whereas in the non-encapsulated condition this value fell to 45%. The morphological analysis of these films by SEM indicated good distribution of the NP in the galactomannan matrix. Thus, the results indicate the feasibility of using the encapsulation method to stabilize vitamin C extracted from the agroindustrial residue of acerola.
机译:从针叶木浆生产中获得的农业工业残留物中富含残留的维生素C。因此,针对其提取和稳定化,这项工作提出了通过离子凝胶化对纳米颗粒(NP)进行封装的方法,并随后制备了基于半乳甘露聚糖基质的纳米复合材料(NC)膜。表征了NP,并在不同的储存条件(光照,温度和氧化性气氛)下评估了它们的稳定性。动态光散射(DLS)和扫描电子显微镜(SEM)的结果表明,形态均匀,球形且尺寸约为220 nm。关于稳定性,紫外可见分光光度法分析显示封装的维生素C的降解率要低得多,与未封装的系统在储存第15天结束时相比,其保存率超过30%。一致的是,NC膜还主要在高温下保存了维生素C,用于高温测试,保持初始浓度的80%,而在非封装条件下,该值降至45%。通过SEM对这些膜进行形态学分析表明,NP在半乳甘露聚糖基质中分布良好。因此,结果表明使用包囊方法稳定从针叶树的农业工业残余物中提取的维生素C的可行性。

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