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Rapid NIR determination of alkyl esters in virgin olive oil

机译:快速近红外光谱法测定初榨橄榄油中烷基酯的含量

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The regulation of The European Union for olive oil and olive pomace established the limit of 35 mg·kg -1 for fatty acids ethyl ester contents in extra virgin olive oils, from grinding seasons after 2016. In this work, predictive models have been established for measuring fatty acid ethyl and methyl esters and to measure the total fatty acid alkyl esters based on near infrared spectroscopy (NIRS), and used successfully for this purpose. The correlation coefficients from the external validation exercises carried out with these predictive models ranged from 0.84 to 0.91. Different classification tests using the same models for the thresholds 35 mg·kg -1 for fatty acid ethyl esters and 75 mg·kg -1 for fatty acid alkyl esters provided success percentages from 75.0% to 95.2%.
机译:欧洲联盟的橄榄油和橄榄果渣法规规定,从2016年以后的研磨季节开始,特级初榨橄榄油中脂肪酸乙酯含量的上限为35 mg·kg -1。在这项工作中,建立了预测模型基于近红外光谱(NIRS)的脂肪酸乙酯和甲基酯的测定以及总脂肪酸烷基酯的测定,已成功用于此目的。使用这些预测模型进行的外部验证练习的相关系数范围为0.84至0.91。使用相同模型的脂肪酸乙酯阈值35 mg·kg -1和脂肪酸烷基酯阈值75 mg·kg -1的不同分类测试,成功率从75.0%到95.2%。

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