Byproduct-Catalyzed Four-Component Reactions of Aldehydes with Hexamethyldisilazane, Chloroformates, and Nucleophiles in Acetonitrile Leading to Protected Primary Amines, β-Amino Esters, and β-Amino Ketones

Bai-Ling Yang Zhen-Tao Weng Si-Jie Yang Shi-Kai Tian Prof. Dr.

首页> 外文期刊>Chemistry - A European Journal >Byproduct-Catalyzed Four-Component Reactions of Aldehydes with Hexamethyldisilazane, Chloroformates, and Nucleophiles in Acetonitrile Leading to Protected Primary Amines, β-Amino Esters, and β-Amino Ketones

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Byproduct-Catalyzed Four-Component Reactions of Aldehydes with Hexamethyldisilazane, Chloroformates, and Nucleophiles in Acetonitrile Leading to Protected Primary Amines, β-Amino Esters, and β-Amino Ketones

机译：乙醛与六甲基二硅氮烷，氯甲酸酯和亲核试剂在副产物催化下的四组分反应导致保护的伯胺，β-氨基酯和β-氨基酮

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来源
《Chemistry - A European Journal》 |2010年第2期|p.718-723|共6页
作者
Bai-Ling Yang Zhen-Tao Weng Si-Jie Yang Shi-Kai Tian Prof. Dr.;
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正文语种 eng
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aldehydes; chloroformates; hexamethyldisilazane; multicomponent reactions; water chemistry;

机译：醛;氯甲酸酯;六甲基二硅氮烷;多组分反应;水化学;

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1. Byproduct-Catalyzed Four-Component Reactions of Aldehydes withHexamethyldisilazane, Chloroformates, and Nucleophiles in Acetonitrile Leading to Protected Primary Amines, b-Amino Esters, and b-Amino Ketones [J] . Bai-Ling Yang, Zhen-Tao Weng, Si-Jie Yang, Chemistry: A European journal . 2010,第2期

机译：乙腈中六价醛与六甲基二硅氮烷，氯甲酸酯和亲核试剂的副产物催化四组分反应，导致被保护的伯胺，b-氨基酯和b-氨基酮
2. Fluoride-catalyzed aldol reaction of ethyl trimethylsilyldiazoacetate with aldehydes leading to ethyl alpha-diazo-beta-hydroxy esters and rhodium catalyzed decarboxylative rearrangement of diazo urethanes leading to beta-amino acrylates [J] . Kanemasa S., Kanai T., Wada E., Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 1999,第27期

机译：氟催化的三甲基硅烷基重氮乙酸乙酯与醛的醛醇缩合反应，生成乙基α-重氮-β-羟基酯，铑催化重氮氨基甲酸酯的脱羧重排，生成β-氨基丙烯酸酯
3. One-pot, four-component reaction of aryl aldehydes, aryl ketones, phosphorus trichloride, and acetonitrile catalyzed by acetyl chloride: Synthesis of beta-acetamido ketones [J] . Anary-Abbasinejad M, Saidipoor A Synthetic Communications . 2008,第1a3期

机译：乙酰氯催化一锅四组分芳基醛，芳基酮，三氯化磷和乙腈的反应：β-乙酰氨基酮的合成
4. Fmoc-beta-Ala-OH and Fmoc-beta-Ala-amino acid-OH:two new impurities in Fmoc-protected amino acid derivatives [C] . Elzbieta Hlebowicz, Jennifer Eriksson, Mikael Nilsson International Peptide Symposium;European Peptide Symposium . 2005

机译：FMOC-BETA-ALA-OH和FMOC-β-ALA-氨基酸-OH：两种新的FMOC保护氨基酸衍生物的杂质
5. Catalytic asymmetric addition reactions leading to carbon-carbon bond formation: Phenyl and alkenyl transfer to aldehydes and alkynylation of alpha-amino ester. [D] . Ji, Jianxin. 2004

机译：催化不对称加成反应，导致形成碳-碳键：苯基和烯基转移至醛类和α-氨基酯的炔基化反应。
6. Photooxidation of d(TpG) by riboflavin and methylene blue. Isolation and characterization of thymidylyl-(35)-2-amino-5-(2-deoxy-beta-D- erythro-pentofuranosyl)amino-4H-imidazol-4-one and its primary decomposition product thymidylyl-(35)-22-diamino-4-(2-deoxy-beta-D- erythro-pentofuranosyl)amino-5(2H)-oxazolone. [O] . G W Buchko, J Cadet, B Morin, 1995

机译：核黄素和亚甲基蓝对d（TpG）的光氧化作用。胸苷基-（35）-2-氨基-5-（2-脱氧-β-D-赤型五氟呋喃糖基）氨基 -4H-咪唑-4-酮及其一次分解产物胸苷基的分离与表征-（35）-22-二氨基-4-（2-脱氧-β-D-赤-五呋喃糖基）氨基 -5（2H）-恶唑酮。
7. The solvent free preparation of beta-amino esters alpha,beta-unsaturated ketones and esters with domestic microwave oven [O] . Mara E. F. Braibante, Hugo T. S. Braibante, Ademir F. Morel, 2006

机译：β-氨基酯的溶剂制备β-氨基酯α，β-不饱和酮和酯用家用微波炉
8. New Application of Bromotrimethylsilane: Elaboration of Aldehydes/ Ketones into Homologous Alpha-Beta-Unsaturated Esters via Beta-Hydroxy Esters [R] . Suri, S. C. , Marcischak, J. C. 2003

机译：Bromotrimethylsilane的新应用：通过β-羟基酯将醛/酮配制成同系的α-β-不饱和酯

Byproduct-Catalyzed Four-Component Reactions of Aldehydes with Hexamethyldisilazane, Chloroformates, and Nucleophiles in Acetonitrile Leading to Protected Primary Amines, β-Amino Esters, and β-Amino Ketones

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