In situ investigation of the oxidative addition in homogeneous Pd catalysts by synchronised time resolved UV-Vis/EXAFS

Guilera G; Newton MA; Polli C; Pascarelli S; Guino M; Hii KK

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In situ investigation of the oxidative addition in homogeneous Pd catalysts by synchronised time resolved UV-Vis/EXAFS

机译：通过同步时间分辨的UV-Vis / EXAFS原位研究均相Pd催化剂中的氧化加成

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摘要

Simultaneous structuro-kinetic information obtained via time resolved stopped-flow/UV-Vis spectroscopy/dispersive EXAFS (EDE) experiments elucidated a two-step process for the addition of iodobenzene to [(Ph3P)(2)Pd(dba)].

机译：通过时间分辨停止流/紫外-可见光谱/分散EXAFS（EDE）实验获得的结构动力学动力学信息同时阐明了将碘代苯添加到[（Ph3P）（2）Pd（dba）]中的两步过程。

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来源
《Chemical Communications》 |2006年第41期|p. 4306-4308|共3页
作者
Guilera G; Newton MA; Polli C; Pascarelli S; Guino M; Hii KK;
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作者单位

European Synchrotron Radiat Facil, F-38043 Grenoble, France;

Univ London Imperial Coll Sci Technol & Med, Dept Chem, London SW7 2AZ, England;

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原文格式 PDF
正文语种 eng
中图分类化学;
关键词
ZEROVALENT PALLADIUM COMPLEXES; PERSONAL ACCOUNT; ARYL HALIDES; C-N; MECHANISM; MIXTURES; PD(DBA)(2); SYSTEMS; LIGAND;

机译：零价钯络合物;个人账户;阿里尔·哈利德斯;C-N;机制;混合物;PD（DBA）（2）;系统;配体;

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机译：镍均相催化剂加三苯基膦和AlEt_2（OEt）作为助催化剂催化的低聚反应的时间分辨能量耗散EXAFS测量
2. Operando spectroscopic investigation of supported metal oxide catalysts by combined time-resolved UV-VIS/Raman/on-line mass spectrometry [J] . T.A.(Xander) Nijhuis, Stan J.Tinnemans, Tom Visser, Physical chemistry chemical physics: PCCP . 2003,第20期

机译：通过时间分辨紫外-可见/拉曼/在线质谱联用技术对负载的金属氧化物催化剂进行操作光谱研究
3. The CO oxidation kinetics on supported Pd model catalysts:A molecular beam/in situ time-resolved infrared reflection absorption spectroscopy study [J] . J.Libuda, I.Meusel, J.Hoffmann, The Journal of Chemical Physics . 2001,第10期

机译：负载型Pd模型催化剂上的CO氧化动力学：分子束/原位时间分辨红外反射吸收光谱研究
4. Temperature-Driven Oxidation Behavior of Pure Iron Surface Investigated by time-resolved EXAFS Measurements [C] . S.J.Doh, J.M.Lee, D.Y.Noh, Symposium on applications of synchrotron radiation techniques to materials science . 1998

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5. Activity, in situ IR and EXAFS spectroscopy studies, and Monte Carlo simulation of the preferential oxidation of carbon monoxide on niobium-promoted platinum/aluminum oxide catalysts and platinum-free metal oxides catalysts. [D] . Guerrero Ruz, Sichem. 2007

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6. Time-Resolved In Situ DRIFTS/EDE/MS Studies on Alumina-Supported Rhodium Catalysts: Effects of Ceriation and Zirconiation on Rhodium–CO Interactions [O] . Anna B Kroner, Mark A Newton, Moniek Tromp, -1

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In situ investigation of the oxidative addition in homogeneous Pd catalysts by synchronised time resolved UV-Vis/EXAFS

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