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首页> 外文期刊>Bulletin of Materials Science >Effect of stabilizer on optical and structural properties of MgO thin films prepared by sol–gel method
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Effect of stabilizer on optical and structural properties of MgO thin films prepared by sol–gel method

机译:稳定剂对溶胶-凝胶法制备的MgO薄膜光学和结构性能的影响

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摘要

The effects of monoethanolamine (MEA) and acetylacetone (ACAC) addition as stabilizer on the crystallization behaviour, morphology and optical properties of magnesium oxide were investigated using thermogravimetry (TG/DTG), X-ray diffraction (XRD), scanning electron microscopy (SEM), UV-Visible, photoluminescence (PL) and Fourier transform infrared (FTIR) spectroscopy. Stabilizer addition reduces transparency of the films. MgO films prepared at 500 °C showed weak orientation of (200). However, the films prepared by addition of stabilizer are amorphous. MgO powders were prepared for exhibiting the structural properties. The patterns of MgO powders showed a preferred orientation of (200). The addition of stabilizer causes a reduction in grain size. SEM micrographs show that a homogenous and crack-free film can be prepared at 500 °C and addition of stabilizer causes an increase in packing density.
机译:用热重法(TG / DTG),X射线衍射(XRD),扫描电子显微镜(SEM)研究了添加单乙醇胺(MEA)和乙酰丙酮(ACAC)作为稳定剂对氧化镁的结晶行为,形貌和光学性质的影响。 ),紫外可见光,光致发光(PL)和傅立叶变换红外(FTIR)光谱。添加稳定剂会降低薄膜的透明度。在500°C下制备的MgO薄膜显示(200)的弱取向。然而,通过添加稳定剂制备的膜是无定形的。制备MgO粉末以表现出结构特性。 MgO粉末的图案显示出优选的取向(200)。添加稳定剂导致晶粒尺寸减小。 SEM显微照片显示,可以在500°C下制备均匀且无裂纹的薄膜,添加稳定剂会导致堆积密度增加。

著录项

  • 来源
    《Bulletin of Materials Science》 |2013年第5期|899-905|共7页
  • 作者

    Z BAZHAN; F E GHODSI; J MAZLOOM;

  • 作者单位

    Department of Physics Faculty of Science University of Guilan">(1);

    Department of Physics Faculty of Science University of Guilan">(1);

    Department of Physics Faculty of Science University of Guilan">(1);

  • 收录信息
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    MgO; thin film; sol–gel; stabilizer;

    机译:氧化镁;薄膜;溶胶凝胶稳定剂;

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