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Synthesis and evaluation of the structural, optical, and antibacterial properties of copper oxide nanoparticles

机译:氧化铜纳米粒子的结构,光学和抗菌性能的合成与评估

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摘要

The nanostructured material, due to their outstanding applications in various fields of science and technology; metal and metal oxide nano are exclusively explored in the progress of nanosized materials. The transition metal oxides including CuO is are used for magnetic storage devices, solar energy applications, sensors, as a catalyst in reactions, as electrode materials in supercapacitors and to tune the semiconducting properties of materials. The current work focuses on the synthesis of CuO nanoparticles (NPs) by combustion technique for various annealing (100 degrees C and 300 degrees C) using ascorbic acid as a capping agent. The XRD pattern confirms that the CuO NPs exhibit the monoclinic structure. The optical properties are investigated using UV-Vis absorption spectra. Further, the refractive index, optical dielectric constant and bulk modulus were investigated using the specific empirical model as a function of temperature. The FTIR spectrum shows that the band in the range 450-500cm(-1) confirms the formation of CuO NPs. The SEM images revealed that the spherical surface morphology of the CuO NPs. The Elemental analysis and the particle size were confirmed by elemental dispersive X-ray analysis (EDX) and particle size analyzer. Moreover, the antibacterial activity of CuO nanoparticles was investigated using E. coli, S. typhi, M. luteus, P. fluorescent, S. flexneri, and V. cholera bacteria.
机译:纳米结构材料,由于其在科学和技术领域的杰出应用;金属和金属氧化物纳米是在纳米材料发展中专门研究的。包括CuO在内的过渡金属氧化物可用于磁存储设备,太阳能应用,传感器,反应中的催化剂,超级电容器中的电极材料以及用于调节材料的半导体性能。当前的工作集中在使用抗坏血酸作为封端剂通过燃烧技术合成CuO纳米颗粒(NPs),以进行各种退火(100摄氏度和300摄氏度)。 XRD图谱证实了CuO NPs具有单斜晶结构。使用UV-Vis吸收光谱研究光学性质。此外,使用特定经验模型作为温度的函数研究了折射率,光学介电常数和体积模量。 FTIR光谱显示450-500cm(-1)范围内的谱带证实了CuO NP的形成。 SEM图像显示了CuO NP的球形表面形态。通过元素色散X射线分析(EDX)和粒度分析仪确认元素分析和粒度。此外,使用大肠杆菌,鼠伤寒沙门氏菌,黄褐藻,荧光球菌,弗氏链球菌和霍乱弧菌研究了CuO纳米粒子的抗菌活性。

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  • 来源
    《Applied Physics 》 |2019年第8期| 489.1-489.9| 共9页
  • 作者单位

    Univ Malaya, Nanotechnol & Catalysis Res Ctr, Kuala Lumpur 50603, Malaysia;

    Jayaraj Annapackiyam Coll Women Autonomous, PG Res Dept Phys, Periyakulam 625605, Tamil Nadu, India;

    Univ Malaya, Nanotechnol & Catalysis Res Ctr, Kuala Lumpur 50603, Malaysia;

    Univ Malaya, Nanotechnol & Catalysis Res Ctr, Kuala Lumpur 50603, Malaysia;

    Univ Malaya, Nanotechnol & Catalysis Res Ctr, Kuala Lumpur 50603, Malaysia;

    Sathyabama Inst Sci & Technol, Dept Phys, Chennai 600119, Tamil Nadu, India;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
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  • 正文语种 eng
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