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首页> 外文期刊>Applied Physics A: Materials Science & Processing >Size And Density Control Of Silicon Oxide Nanowires By Rapid Thermal Annealing And Their Growth Mechanism
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Size And Density Control Of Silicon Oxide Nanowires By Rapid Thermal Annealing And Their Growth Mechanism

机译:快速热退火控制氧化硅纳米线的尺寸和密度及其生长机理

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摘要

In this work, we demonstrate a fast approach to grow SiO_2 nanowires by rapid thermal annealing (RTA). The material characteristics of SiO_2 nanowires are investigated by field emission scanning electron microscopy, high-resolution transmission electron microscopy (HRTEM), high-angle annular dark-field (HAADF) imaging, electron energy loss spectroscopy (EELS), and energy-filtered TEM (EFTEM). The HAADF images show that the wire tip is predominantly composed of Pt with brighter contrast, while the elemental mappings in EFTEM and EELS spectra reveal that the wire consists of Si and O elements. The SiO_2 nanowires are amorphous with featureless contrast in HRTEM images after RTA at 900℃. Furthermore, the nanowire length and diameter are found to be dependent on the initial Pt film thickness. It is suggested that a high SiO_2 growth rate of > 1 μm/min can be achieved by RTA, showing a promising way to enable large-area fabrication of nanowires.
机译:在这项工作中,我们演示了一种通过快速热退火(RTA)生长SiO_2纳米线的快速方法。通过场发射扫描电子显微镜,高分辨率透射电子显微镜(HRTEM),高角度环形暗场(HAADF)成像,电子能量损失谱(EELS)和能量过滤TEM研究SiO_2纳米线的材料特性(EFTEM)。 HAADF图像显示焊丝尖端主要由具有更亮对比度的Pt组成,而EFTEM和EELS光谱中的元素映射显示焊丝包含Si和O元素。 SiO_2纳米线是非晶态的,在900℃RTA后,HRTEM图像中对比度没有明显变化。此外,发现纳米线的长度和直径取决于初始Pt膜的厚度。建议通过RTA可以实现> 1μm/ min的高SiO_2生长速率,这显示了实现纳米线大面积制造的有前途的方法。

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