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Preparation and Characterization of Chitosan Poly(acrylic acid) Magnetic Microspheres

机译:壳聚糖聚丙烯酸磁性微球的制备与表征

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摘要

Spherical microparticles, capable of responding to magnetic fields, were prepared by encapsulating dextran-coated Fe3O4 nanoparticles into chitosan poly(acrylic acid) (PAA) microspheres template. The obtained magnetic microspheres were characterized by transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray powder diffraction (XRD), and thermogravimetry (TG). The results showed that the microspheres were formed and demonstrated magnetic behavior in an applied magnetic field. In addition, magnetite particles were well encapsulated and the composite particles have high magnetite content, which was more than 40%.
机译:通过将葡聚糖包被的Fe3O4纳米颗粒封装到壳聚糖聚丙烯酸(PAA)微球模板中,制备了能够响应磁场的球形微粒。通过透射电子显微镜(TEM),傅立叶变换红外光谱(FT-IR),扫描电子显微镜(SEM),X射线粉末衍射(XRD)和热重分析(TG)表征获得的磁性微球。结果表明,形成了微球并在施加的磁场中表现出磁行为。另外,磁铁矿颗粒被很好地包封并且复合颗粒具有高的磁铁矿含量,其超过40%。

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