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Absence of dynamic strain aging in an additively manufactured nickel-base superalloy

机译:增材制造的镍基高温合金中没有动态应变时效

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摘要

Dynamic strain aging (DSA), observed macroscopically as serrated plastic flow, has long been seen in nickel-base superalloys when plastically deformed at elevated temperatures. Here we report the absence of DSA in Inconel 625 made by additive manufacturing (AM) at temperatures and strain rates where DSA is present in its conventionally processed counterpart. This absence is attributed to the unique AM microstructure of finely dispersed secondary phases (carbides, N-rich phases, and Laves phase) and textured grains. Based on experimental observations, we propose a dislocation-arrest model to elucidate the criterion for DSA to occur or to be absent as a competition between dislocation pipe diffusion and carbide–carbon reactions. With in situ neutron diffraction studies of lattice strain evolution, our findings provide a new perspective for mesoscale understanding of dislocation–solute interactions and their impact on work-hardening behaviors in high-temperature alloys, and have important implications for tailoring thermomechanical properties by microstructure control via AM.
机译:长期以来,在高温下塑性变形的镍基高温合金中,普遍观察到动态应变时效(DSA)呈锯齿状塑性流动。在这里,我们报告了Inconel 625中不存在通过增材制造(AM)在温度和应变率下制造的DSA的情况,其中DSA存在于其常规加工的对应物中。这种缺乏归因于精细分散的第二相(碳化物,富氮相和Laves相)和织构晶粒的独特AM微结构。根据实验观察,我们提出了位错-阻滞模型,以阐明位错管扩散与碳化物-碳反应之间的竞争而导致DSA发生或不存在的标准。通过对晶格应变演化的原位中子衍射研究,我们的发现为中尺度理解位错-溶质相互作用及其对高温合金中加工硬化行为的影响提供了新的视角,并且对于通过微结构控制来调整热机械性能具有重要意义。通过AM。

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