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Preparation and Characteristics of TiO2 Photocatalyst Loaded onto the Attapulgite Clay

机译:凹凸棒土上负载TiO2光催化剂的制备与性能研究。

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In order to investigate the effects of photocatalysis technique to the wastewater of dye, a new carrier of catalyst--micron attapulgite clay was selected. The TiO2/attapulgite clay photocatalyst was prepared by the sol-gel method. X-ray diffraction indicates that its diffracted peak of surface is same as the characteristic peak of TiO2. SEM pictures showed the form of sample is amorphous, and the diameter of the particle is between 1 and 5 μm. The photo catalytic activity of TiO2/attapulgite clay was studied in a device with ultraviolet lamp as light source and methylene blue as the substrate With other conditions unchanged, the less the pH value, the lower the concentration of methylene blue, the higher decolorizing rate of the substrate. During the limited range the amount of catalyst has a great effect on the discoloration while the temperature and aeration volume slightly affect it. Within 30 minutes, the decolorizing rate of methylene blue reaches over 90%, this is one fold higher than the result just with single TiO2.
机译:为了研究光催化技术对染料废水的影响,选择了一种新型的催化剂载体-微米级凹凸棒粘土。采用溶胶-凝胶法制备了TiO2 /凹凸棒石粘土光催化剂。 X射线衍射表明其表面的衍射峰与TiO 2的特征峰相同。 SEM照片显示样品的形式是无定形的,并且颗粒的直径在1-5μm之间。以紫外灯为光源,以亚甲基蓝为底物的装置研究了TiO2 /凹凸棒石粘土的光催化活性。在其他条件不变的情况下,pH值越小,亚甲基蓝的浓度越低,脱色率越高。基板。在有限的范围内,催化剂的量对变色有很大的影响,而温度和通气量对变色的影响很小。在30分钟内,亚甲基蓝的脱色率达到90%以上,比仅使用TiO2的结果高一倍。

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