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Compressive and wear resistance of alumina reinforced Fe-Cr matrix Composites

机译:氧化铝增强Fe-CR基复合材料的压缩和耐磨性

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Fe-Cr matrix composite reinforced with alumina with mean powder sizes of 13, 23, 24 and 64μm was successfully obtained through powder metallurgy method. The powder mixture were blended at a rotating speed of 250 rpm for thirty minutes and uni-axially pressed at a pressure of 750 MPa. Samples identified as J13, J23, J24 and J64 according to alumina particles size were sintered in a vacuum furnace under 10~(-2) Torr at a temperature of 1100°C for two hours with 10°C/minutes heating rate. The peaks of XRD patterns have been identified as belonging to the phases of Fe, Cr and alumina. The EDX analysis confirms the existence of Fe, Cr, Al and O. Reinforcing the Fe-Cr matrix with alumina particles bigger than 13μm deteriorated the microstructure and mechanical properties of the composites. The wear coefficient for sample reinforced with 13μm alumina particles is 2.46 × 10~(-11) with compressive strength of 278 MPa. Meanwhile for sample reinforced with 64μm alumina particles its wear coefficient is 5.09 × 10~(-11) and compressive strength is 81 MPa. It is found that reinforcing smaller alumina particles sizes to Fe-Cr matrix resulted in better wear and strength properties of the composites.
机译:通过粉末冶金方法成功地获得含有13,23,24和64μm的平均粉末尺寸的氧化铝的Fe-Cr基质复合材料。将粉末混合物以250rpm的旋转速度混合30分钟,并且在750MPa的压力下单轴压制。根据氧化铝颗粒尺寸鉴定为J13,J23,J24和J64的样品在10℃/分钟的温度下在10℃/分钟的温度下在10℃/分钟的温度下在10〜(2)托的真空炉中烧结。 XRD模式的峰已被鉴定为属于Fe,Cr和氧化铝的阶段。 EDX分析证实Fe,Cr,Al和O.用大于13μm的氧化铝颗粒加固Fe-Cr基质劣化复合材料的微观结构和机械性能。用13μm氧化铝颗粒加固的样品的磨损系数为2.46×10〜(-11),抗压强度为278MPa。同时对于用64μm氧化铝颗粒加固的样品,磨损系数为5.09×10〜( - 11),抗压强度为81MPa。发现加强较小的氧化铝颗粒尺寸至Fe-Cr基质,导致复合材料的磨损和强度性质。

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