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Preparation and Superparamagnetic Properties of graphene/Fe_3O_4 Nanocomposite

机译:石墨烯/ Fe_3O_4纳米复合材料的制备和超顺磁性性能

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The superparamagnetic graphene/Fe_3O_4 nanocomposite has been successfully prepared via an easy and scalable chemical precipitation method. High quality graphene sheets were prepared from natural flake graphite by oxidation, rapid expansion and ultrasonic treatment. The structure of graphene and graphene/Fe_3O_4 nanocomposite was investigated by transmission electron microscopy, X-ray diffraction and Fourier transform infrared spectroscopy. The graphene sheets possess a curled morphology consisting of a thin wrinkled paper-like structure. The graphene/Fe_3O_4 nanocomposite exhibits a superparamagnetic behavior, its specific saturation magnetization, Ms is 38.92 emug~(-1).
机译:通过简单且可伸缩的化学沉淀法成功制备了超顺磁性石墨烯/ Fe_3O_4纳米复合材料。通过氧化,快速膨胀和超声处理由天然薄片石墨制备优质石墨烯片。通过透射电子显微镜,X射线衍射和傅里叶变换红外光谱研究了石墨烯和石墨烯/ Fe_3O_4纳米复合材料的结构。石墨烯片具有由薄皱的纸状结构组成的卷曲形态。石墨烯/ Fe_3O_4纳米复合材料表现出超顺磁性行为,其特定的饱和磁化强度,MS为38.92倍〜(-1)。

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