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IN-SITU BRAGG COHERENT X-RAY DIFFRACTION DURING TENSILE TESTING OF AN INDIVIDUAL AU NANOWIRE

机译:在单独的Au纳米线的拉伸测试过程中原位布拉格相干X射线衍射

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Nanomechanical testing methods have drawn significant attention in both scientific and industrial research fields owing to unique deformation mechanisms in constrained volumes that underpin new property regimes. In-situ imaging equipment is now routinely employed to monitor the live evolution of material response during mechanical loading, with many of the testing developments tailored for electron microscopes (EMs). More recently, progress towards quantitative in-situ testing at synchrotron beamlines enabled by innovations in source brightness, focusing optics, and large size detectors has been made. Novel techniques such as Bragg coherent X-ray diffraction promise 3D information with phase information related to displacement fields (elastic strain, defects) within the material. However, despite the rich information that can be collected, many challenges arise in the realization of in-situ imaging of single nanostructures using such methods, including meticulous sample preparation and complex data analysis in retrieving phase information.
机译:由于受限制卷的独特变形机制,纳米力学检测方法在科学和工业研究领域造成了严重的关注,这是基于新的财产制度的受约束卷的独特变形机制。现场成像设备现在通常用于监测机械负载期间材料响应的实时演变,许多用于电子显微镜(EMS)的测试开发。最近,已经制作了通过源亮度,聚焦光学元件和大尺寸探测器的创新实现的同步辐射线线路上定量原位测试的进展。诸如布拉格相干X射线衍射的新技术,其具有与材料内的位移场(弹性应变,缺陷)相关的相位信息的3D信息。然而,尽管可以收集丰富的信息,但在使用这种方法实现单个纳米结构的原位成像时出现了许多挑战,包括在检索相信息中的细致样品制备和复杂的数据分析。

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