Optimization of Progressive Freeze Concentration on Apple Juice via Response Surface Methodology

摘要

In this work,a progressive freeze concentration(PFC)system was developed to concentrate apple juice and was optimized by response surface methodology(RSM).The effects of various operating conditions such as coolant temperature,circulation flowrate,circulation time and shaking speed to effective partition constant(K)were investigated.Five different level of central composite design(CCD)was employed to search for optimal concentration of concentrated apple juice.A full quadratic model for K was established by using method of least squares.A coefficient of determination(R~2)of this model was found to be 0.7792.The optimum conditions were found to be coolant temperature =-10.59 °C,circulation flowrate = 3030.23 mL/min,circulation time = 67.35 minutes and shaking speed = 30.96 ohm.A validation experiment was performed to evaluate the accuracy of the optimization procedure and the best K value of 0.17 was achieved under the optimized conditions.