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Investigation of Structural and Antifungal Behaviors of Nano-Sized Anatase Titanium Dioxide Synthesized by Co-Precipitation Route

机译:共析出路径合成纳米锐钛矿二氧化钛结构和抗真菌行为的研究

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Nowadays, the application of nano-sized anatase titanium dioxide particles becomes one of the essential research focuses by many experts, especially for biomedical applications. In this work, we report the utilization of coprecipitation route in preparing nano-sized anatase titanium dioxide as an antifungal agent. The data analysis for the XRD data of the titanium dioxide particles showed that the sample crystallized with anatase structure and sized in the nanometric size of 13.30 nm. The particle size obtained from Scherrer's analysis of the XRD data was quite similar to the particle size obtained from electron microscopy investigation. Furthermore, the small-angle scattering data presented that the anatase titanium dioxide constructed a 3-dimensional structure with a compact structure originating from the fractal dimension value of approximately 3. The functional groups of the nano-sized anatase titanium dioxide were traced in the wavelength range of 500-1500 cm~(-1) showing the presence of Ti-0 bonding. Interestingly, the prepared sample in this experiment exhibited an excellent performance as an antifungal agent represented by inhibition zone diameter of 3.59 mm.
机译:如今,纳米大小的锐钛矿二氧化钛颗粒的应用成为许多专家的基本研究之一,特别是对于生物医学应用。在这项工作中,我们报告了在制备纳米沉淀酶作为抗真菌剂中的纳米沉淀酶钛的用途。二氧化钛颗粒的XRD数据的数据分析表明,样品用锐钛矿结构结晶并占纳米尺寸为13.30nm。从Scherrer对XRD数据分析获得的粒度非常类似于从电子显微镜调查获得的粒度。此外,小角度散射数据呈现,锐钛矿二氧化钛构造了三维结构,其具有源于大​​约3.纳米型锐钛矿钛的分形尺寸值​​的紧凑结构。在波长中追踪纳米尺寸的锐钛矿钛的二氧化钛的官能团500-1500cm〜(-1)的范围显示Ti-0键合的存在。有趣的是,该实验中制备的样品表现出优异的性能,作为抑制区直径为3.59mm的抗真菌剂。

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