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Thermoluminescence properties of TiO_2 nanoparticles synthesized using co-precipitation method

机译:使用共沉淀法合成的TiO_2纳米粒子的热致发光性能

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In the present study, Titanium dioxide (TiO_2) nanoparticles have been synthesised using co-precipitation technique using titanium tetrachloride and sodium hydroxide as a precursor materials. The TiO_2 nanoparticles so obtained were characterized using powder X-ray Diffraction (XRD) and Scanning Electron Microscopy (SEM) for structural and morphological properties. The TiO_2 nanoparticles were annealed at 450°C, 500°C, and 550°C. The synthesised compounds were irradiated with gamma radiation ranging from 200 Gy to 1 kGy. Thermoluminescentand dosimetric characteristics of TiO_2 nanoparticles have been studied using Thermoluminescent Dosimeter (TLD) reader (Model No: 1009I). The thermoluminescence (TL) glow curves of TiO_2 nanoparticles have been evaluated for different doses of gamma irradiation. The TL response of these nanoparticles shows the increasing trend with increasing of annealing temperature. The more detailed analysis along with results and discussions are presented in this paper.
机译:在本研究中,已经使用使用四氯化钛和氢氧化钠作为前体材料合成二氧化钛(TiO_2)纳米颗粒。如此获得的TiO_2纳米颗粒用粉末X射线衍射(XRD)和扫描电子显微镜(SEM)表征,用于结构和形态学性质。将TiO_2纳米颗粒在450℃,500℃和550℃下退火。用200GY至1kGy的γ辐射照射合成的化合物。使用热致敏剂量计(TLD)读取器研究了TiO_2纳米颗粒的热醇细胞剂量特性(型号:1009i)。已经评估了TiO_2纳米颗粒的热致发光(TL)辉光曲线,用于不同剂量的γ辐射。这些纳米颗粒的T1响应显示出增加退火温度的趋势。本文提出了更详细的分析和讨论。

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