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Wear behavior of electroless Ni-P coatings in brine solution and optimization of coating parameters

机译:盐水溶液中电镀Ni-P涂层的磨损行为及涂层参数优化

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The present paper studies the wear behavior of electroless Ni-P coating in brine medium and optimization of the coating process parameters for minimum wear using Taguchi method based on L27 orthogonal array. The study is carried out using different combinations of four coating process parameters, namely, concentration of nickel source (A), concentration reducing agent (B), bath temperature (C) and annealing temperature (D). The wear tests are conducted with a pin-on-disk Wear & Friction Monitor. The optimum combination of process parameters for minimum depth of wear is obtained. ANOVA is performed to find out the significance of the coating parameters and their interactions. The surface morphology and composition of coatings are studied with the help of scanning electron microscopy (SEM), energy dispersed X-ray (EDX) analysis and X-ray diffraction (XRD) analysis. It is found that Ni-P coating is amorphous in as-deposited condition but gradually turns crystalline with heat treatment. The worn surface morphology reveals abrasive as well as corrosive wear mechanism.
机译:本文研究了基于L27正交阵列的Taguchi方法的盐水介质中电镀Ni-P涂层的磨损行为,并使用基于L27正交阵列的Taguchi方法的涂布工艺参数的优化。该研究采用不同组合的四种涂布工艺参数,即浓度的镍源(A),浓度还原剂(B),浴温(C)和退火温度(D)进行。磨损试验用销磁盘磨损和摩擦监测器进行。获得了用于最小磨损深度的工艺参数的最佳组合。进行ANOVA以了解涂层参数及其相互作用的重要性。利用扫描电子显微镜(SEM),能量分散的X射线(EDX)分析和X射线衍射(XRD)分析来研究涂料的表面形态和组成。发现Ni-P涂层在沉积条件下是无定形的,但逐渐与热处理变成结晶。磨损的表面形态显示出磨料以及腐蚀性磨损机制。

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