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Synthesis and Characterization of Carbon Nanotubes from Natural Source - Camphor Oil

机译:自然源碳纳米管的合成与表征 - 樟脑油

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Carbon nanotubes (CNTs) were deposited on silicon wafer (Si) by Thermal Chemical Vapor Deposition (TCVD). The new starting material of camphor oil was used as carbon precursor. The gas flow of Argon (Ar) was constant at 100 bubbles per minute and 30 minutes of deposition time. Before the deposition process, silicon was coated with mixture of nickel (II) nitrate hexahydrate, Ni (NO_3)_2·6H_2O and ethyl alcohol, C_2H_5OH using spin coater. Variable parameter which is deposition temperature has been studied. Chemical functional groups of carbon nanotubes were characterized using FTIR while surface morphology and uniformity were characterized using FESEM. The FTIR result shows peaks attributed to multi-walled carbon nanotubes (MWCNT) vibration modes.
机译:通过热化学气相沉积(TCVD)在硅晶片(Si)上沉积碳纳米管(CNT)。樟脑油的新原料用作碳前体。氩气(Ar)的气体流动在100个/分钟的沉积时间和30分​​钟的沉积时间恒定。在沉积过程之前,硅涂有镍(II)硝酸己二醇的混合物,Ni(NO_3)_2·6H_2O和乙醇,使用旋涂机C_2H_5OH。研究了沉积温度的可变参数。使用FESEM使用FTIR,使用FTIR表征化学官能团的碳纳米管的特征在于使用FESEM表征表面形态和均匀性。 FTIR结果显示归因于多壁碳纳米管(MWCNT)振动模式的峰值。

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