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Characterization of TiAlBN Nanocomposite Coating deposited via Radio Frequency Magnetron Sputtering using Single Hot-Pressed Target

机译:单一热压靶通过射频磁控溅射沉积的TiAlbn纳米复合涂层的表征

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TiAlBN coatings have been deposited at varying bias voltage of 0, -60, and -150 V by radio frequency (RF) magnetron sputtering technique. A single hot-pressed Ti-Al-BN target was used for the deposition process. With glancing angle X-ray diffraction analysis (GAXRD), the nanocrystalline (nc-) (Ti,Al)N phase was identified. In addition, the existence of BN and TiB_2 amorphous (a-) phase were detected by X-ray photoelectron spectroscopy (XPS) analysis. Thus, the deposited TiAlBN coatings were confirmed as nc-(Ti,Al)N/a-BN/a-TiB_2 nanocomposite. On the other hand, it was found that optimum bias voltage used in present study is -60 V where the deposited TiAlBN coating exhibits an excellent adhesion quality. The adhesion quality of the coatings deposited at -60 V bias voltage is classified as HF 1 evaluated using the Rockwell-C adhesion test method (developed by the Union of German Engineers).
机译:通过射频(RF)磁控溅射技术,在0,-60和-150V的变化偏置电压下沉积TiAlbn涂层。单个热压的Ti-Al-BN靶用于沉积过程。通过透明角X射线衍射分析(GAXRD),鉴定纳米晶(NC-)(Ti,Al)N相。另外,通过X射线光电子能谱(XPS)分析检测BN和TIB_2非晶(A-)相的存在。因此,将沉积的TiAlBN涂层证实为NC-(Ti,Al)N / A-BN / A-Tib_2纳米复合材料。另一方面,发现本研究中使用的最佳偏置电压为-60V,其中沉积的TiAlbn涂层具有出色的粘合品质。沉积在-60V偏置电压下的涂层的粘附质量被分类为使用Rockwell-C粘附测试方法(由德国工程师联盟开发)评估的HF 1。

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