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Investigation of the Crystalline Orientations and Substrates Dependence on Mechanical Properties of PZT Thin Films by Nanoindentation

机译:纳米茚满的晶体取向和基材依赖于PZT薄膜力学性能的研究

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In this paper, we investigated the effects of the substrates and crystalline orientations on the mechanical properties of Pb(Zr_(0.52)Ti_(0.48))O_3 thin films. The PZT thin films were deposited by sol-gel method on platinized silicon substrates with different types of layer materials such as silicon nitride and silicon oxide. The crystalline orientations of PZT thin films were controlled by combined parameters of a chelating agent and pyrolysis temperature. A nanoindentation CSM (continuous stiffness measurement) technique was employed to characterize the mechanical properties of those PZT thin films. It was observed that (001/100)-oriented films show a higher Young's modulus compared to films with mixed orientations of (110) and (111), indicating a clear dependence on film orientation. The influence of substrates on the mechanical properties of PZT thin films was also characterized. Finally, no significant influence of the film thickness was found on the mechanical properties of films thicker than 200 nm.
机译:在本文中,我们研究了基材和结晶取向对Pb的机械性能的影响(Zr_(0.52)Ti_(0.48))O_3薄膜。通过溶胶 - 凝胶法在具有不同类型的层材料如氮化硅和氧化硅的镀层材料上沉积PZT薄膜。 PZT薄膜的结晶取向由螯合剂和热解温的组合参数控制。使用纳米凸缘CSM(连续刚度测量)技术来表征那些PZT薄膜的机械性能。观察到(001/100) - 与具有(110)和(111)的混合取向的薄膜相比,较高的杨氏模量显示出更高的杨氏模量,表明对膜取向的清晰依赖性。底物对PZT薄膜的力学性能的影响还表征。最后,在厚度小于200nm的薄膜的机械性能下没有发现薄膜厚度的显着影响。

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