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ANALYSIS OF METAL OXIDE DEPOSITION ON THE SURFACEOF SiCPARTICLE BY ELECTROLESS PLATING ON Al/ SiC_pCOMPOSITE

机译:Al / SiC_pcomposite用电镀晶体粒子表面上的金属氧化物沉积分析

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Electroless plating are used to coat SiC particles as reinforcement to produce Al/SiC_p metalmatrix composites by powder metallurgy method. Nitride Acid (HNO_3), aluminum andmagnesium were used in solutions to coat the surface of SiC particles by metal oxidedeposition. The magnesium was added 0.02 and 0.25 grams into the solution. The coatinglayer will improve the wetting system between Al and SiC. Aluminum and SiC coated powderwere compacted at pressure of 15 kN, then sintered at 600°C for 2, 4 and 6 hours. All samplesthen were characterized both mechanical properties and microstructural analysis. It isobserved that metal oxide deposition with 0.02 gram of Mg was more homogeneous than 0.25gram of Mg. The microstructures of SiC-coated is analysed by high resolution of scanning electron microscope (SEM) and X-ray Diffraction (XRD). The results show that a metal oxide- substrate bonding action takes place during plating and XRD confirm that spinal phases are found during sintering. The compatibility of Al/SiCp composite which reinforced by SiC coating increased. The compressive strength increased after sintering at 600°C for 6 hours. This is evident that electroless metal oxide deposition on SiC_p particles plays an important role in increasing adhesion strength between the SiC particles and matrix aluminum to produce Al/SiC_p composites.
机译:化学镀层用于通过粉末冶金方法涂覆SiC颗粒作为增强件以产生Al / SiC_P Metalmatrix复合材料。氮化酸(HNO_3),铝andMagnesium用于溶液中通过金属氧沉积涂覆SiC颗粒的表面。向溶液中加入0.02和0.25克的镁。涂层层将改善Al和SiC之间的润湿系统。铝和SiC涂层粉末在15kn压力下压实,然后在600℃下烧结2,4和6小时。所有Samplesthen都表征了机械性能和微观结构分析。它以0.22克Mg的金属氧化物沉积比0.25克的Mg更均匀。通过扫描电子显微镜(SEM)和X射线衍射(XRD)的高分辨率分析SiC涂层的微观结构。结果表明,在电镀和XRD期间进行金属氧化物基质键合作用,确认在烧结期间发现脊髓阶段。通过SiC涂层加固的Al / SiCP复合材料的相容性增加。在600℃下烧结6小时后抗压强度增加。显而易见的是,在SiC_P颗粒上的无电金属氧化物沉积在增加SiC颗粒和基质铝之间的粘合强度以产生Al / SiC_P复合材料的作用中起重要作用。

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