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Effects of growing conditions on preparation of InSb thin films by femtosecond pulsed laser deposition

机译:生长条件对Femtosecond脉冲激光沉积的INSB薄膜制备的影响

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A series of InSb thin films were fabricated on the sapphire substrate by femtosecond pulsed laser deposition (fsPLD) method with the laser of 110 fs pulse width. The laser incident energy is near 1mJ. The target is one kind of heavily doped n-type InSb. The substrate temperature changes from 80 oC to 400 oC, Laser frequency changes from 1 Hz to 1 kHz and laser energy density changes from 0.1 J/cm~2 to 1 J/cm~2. The effects of different laser frequencies, substrate temperature and laser energy density on the surface morphology and optical property have been investigated separately. The surface morphology of InSb thin films was observed by metallurgical microscope and scanning electron microscope (SEM). The thin film with better surface morphology is obtained when the laser frequency is 10 Hz, substrate temperature is 80 oC and laser energy density is 0.1 J/cm~2. X-ray diffraction (XRD) demonstrates that the InSb thin film has a good single crystal structure. The infrared transmittance of InSb thin films is measured by an infrared spectrometer. The results show that good InSb thin films can be prepared by fsPLD. It is found that the mid-wavelength Infrared transmission through the InSb thin films is near 55% and it almost does not change under the different growing conditions.
机译:通过Femtosecond脉冲激光沉积(FSPLD)方法在蓝宝石衬底上制造了一系列INSB薄膜,其激光器为110 FS脉冲宽度。激光入射能量接近1MJ。目标是一种掺杂的n型Insb。基板温度从80℃变化到400℃,激光频率从1 Hz变为1 kHz,激光能量密度从0.1J / cm〜2到1J / cm〜2的变化。分别研究了不同激光频率,衬底温度和激光能量密度对表面形态和光学性能的影响。通过冶金显微镜和扫描电子显微镜(SEM)观察INSB薄膜的表面形态。当激光频率为10Hz时,获得具有更好表面形态的薄膜,衬底温度为80℃,激光能量密度为0.1J / cm〜2。 X射线衍射(XRD)表明INSB薄膜具有良好的单晶结构。通过红外光谱仪测量INSB薄膜的红外透射率。结果表明,良好的INSB薄膜可以通过FSPLD制备。结果发现,通过INSB薄膜的中波长红外传输接近55%,在不同的生长条件下几乎不会改变。

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